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Development of a unidirectional cooling technique for synthesizing compound semiconductors in 10 m drop tower

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Abstract

The solidification process and structures of CdTe solidified in microgravity were studied using the unidirectional cooling apparatus in a 10 m drop tower. Since the drop tower provides 1.4 seconds of microgravity, the unidirectional cooling apparatus cools samples rapidly by cooling gas. The system adopts a Pt heater, which accurately heats samples to a maximum of 1300°C. The sample is placed in an ampoule under vacuum conditions. A flat wall in the ampoule divides the inner sealed sample from the outer open side. A nozzle blowing cooling gas is directed on to the outer wall, and cools the sample until solidification. The cooling properties were measured during CdTe solidification in microgravity. The result shows that solidification occurred between 0.9 and 1.3 seconds after release, so solidification is completed in microgravity. Optical microscope (OM) observation of the sample solidified in microgravity revealed that it produces CdTe and Te phases with segregation patterns, and the structures are ordered along the cooling direction, whereas no order is observed in the structures of the terrestrial sample solidified under 1 g.

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Authors and Affiliations

  1. National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba Central 5, 1-1-1 Higashi, Tsukuba, 305-8565, Ibaraki, Japan

    Mikito Mamiya, Takashi Tsurue, Hiroyuki Miyazaki & Takeshi Okutani

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  1. Mikito Mamiya
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  2. Takashi Tsurue
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  3. Hiroyuki Miyazaki
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  4. Takeshi Okutani
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Correspondence to Mikito Mamiya.

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Mamiya, M., Tsurue, T., Miyazaki, H. et al. Development of a unidirectional cooling technique for synthesizing compound semiconductors in 10 m drop tower. Microgravity Sci. Technol 15, 13–17 (2004). https://doi.org/10.1007/BF02870954

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  • DOI: https://doi.org/10.1007/BF02870954

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