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Determination of UV-absorbing anions in environmental samples by microcolumn high-performance liquid chromatography

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Abstract

The Chromatographic retention and separation of NO -2 , Br-, NO -3 , and I- anions on a column packed with Nucleosil 100-5 C18 dynamically modified with trimethyloctadecylammonium bromide (TMODAB) was studied using direct UV detection. A procedure was developed for the determination of the above anions in the concentration range 0.06-2500 Μg/L without preconcentration. Sample preparation involved only the elimination of organic impurities (if present) from the test sample. The procedure was used for the determination of NO -2 and NO -3 anions in Baikal Lake water and in an aerosol extract.

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Authors and Affiliations

  1. Russian Academy of Sciences, Institute of Limnology, Siberian Division, UlanBatorskaya ul. 3, 664033, Irkutsk, Russia

    A. L. Vereshchagin, V. F. Dudinskii, L. P. Golobokova, G. I. Baram & M. A. Grachev

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  1. A. L. Vereshchagin
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  2. V. F. Dudinskii
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  3. L. P. Golobokova
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  4. G. I. Baram
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  5. M. A. Grachev
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Vereshchagin, A.L., Dudinskii, V.F., Golobokova, L.P. et al. Determination of UV-absorbing anions in environmental samples by microcolumn high-performance liquid chromatography. J Anal Chem 55, 1000–1002 (2000). https://doi.org/10.1007/BF02756095

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  • DOI: https://doi.org/10.1007/BF02756095

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