Abstract
A single-stage closed-cycle helium gas cryogenerator, capable of cooling between 77 K and 300 K, has been installed on the 4-circle neutron diffractometer at CIRUS. The cryo-tip assembly has been incorporated directly on the ϕ-circle of the full-circle crystal orienter in place of the goniometer head used in room temperature experiments. The salient features of this low-temperature attachment and its performance are discussed.
Similar content being viewed by others
References
Agron P A, Levy H A and Bogardus B J 1972J. Appl. Crystallogr. 5 432
Allibon J R, Filhol A, Lehmann M S, Mason S A and Simms P 1981J. Appl. Crystallogr. 14 326
Bhakay-Tamhane S and Sequeira A 1986Ferroelectrics 69 241
Burbank R D 1973J. Appl. Crystallogr. 6 437
Coppens P, Ross F K, Blessing R H, Cooper W F, Larsen F K, Leipoldt J G, Rees B and Leonard R 1974J. Appl. Crystallogr. 7 315
Khan D C and Erickson R A 1970Rev. Sci. Instrum. 41 107
Lippman R and Rudman R 1976J. Appl. Crystallogr. 9 220
Rudman R 1976‘Low temperature x-ray diffraction’: Monographs in low-temperature physics (New York: Plenum)
Sequeira A, Momin S N, Rajagopal H, Soni J N, Chidambaram R, Dilip Kumar, Ramana Rao A and Gopu V M 1978Pramana-J. Phys. 13 223
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Sequeira, A., Bhakay-Tamhane, S. & Sawant, S.R. A low-temperature attachment for a four-circle neutron diffractometer. Bull. Mater. Sci. 8, 591–595 (1986). https://doi.org/10.1007/BF02744360
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF02744360