Abstract
A simple hydrothermal cell without threaded parts has been developed for routine synthesis of materials at moderate temperatures (upto 500°C) and pressures (upto 5 kb). The sealing of the fluid pressure in the cell has been achieved with a cone-seat arrangement, but the sealing pressure has been through a hydraulic ram instead of a threaded cap. Experience showed that this cell is more convenient for rapid and routine experimentation.
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Tareen, J.A.K., Basavalingu, B., Shankara, M.A. et al. A simple hydrothermal cell for synthesis at moderate temperatures and pressures. Bull. Mater. Sci. 8, 543–546 (1986). https://doi.org/10.1007/BF02744353
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DOI: https://doi.org/10.1007/BF02744353