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Synthesis and structural characterization of CsNiP crystal

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Abstract

CsNiP crystals were synthesized by hydrothermal technique and characterized by the X-ray diffraction method. This alkaline transition metal phosphide crystallizes in the hexagonal system with space groupP6 3/mmc and cell parameters,a = 7.173(2) Å,c = 5.944(9) Å,V = 264.87(7) Å3 andZ = 2. The final residual factor isR1 = 0.0362 for 206 reflections withI > 2σ(I).

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Authors and Affiliations

  1. Department of Studies in Geology, University of Mysore, 570 006, Manasagangotri, Mysore, India

    G. S. Gopalakrishna, B. H. Doreswamy, M. J. Mahesh, M. Mahendra, M. A. Sridhar, J. Shashidhara Prasad & K. G. Ashamanjari

  2. Department of Studies in Physics, University of Mysore, 570 006, Manasagangotri, Mysore, India

    B. H. Doreswamy, M. Mahendra, M. A. Sridhar & J. Shashidhara Prasad

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  1. G. S. Gopalakrishna
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  2. B. H. Doreswamy
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  3. M. J. Mahesh
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  6. J. Shashidhara Prasad
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Gopalakrishna, G.S., Doreswamy, B.H., Mahesh, M.J. et al. Synthesis and structural characterization of CsNiP crystal. Bull Mater Sci 27, 27–30 (2004). https://doi.org/10.1007/BF02708480

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