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Optimization by orthogonal array design of solid phase extraction of organochlorine pesticides from water

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Summary

A two-level orthogonal array design (OAD) to optimize the solid phase extraction of organochlorine pesticides is described. Parameters including eluting solvents, SPE cartridges packed with C18-bonded silica from different manufacturers, duration of air drying, pH, salinity and humic acid have been examined using OAD. This systematic approach was then used to optimize the relevant parameters required for off-line solid phase extraction of organochlorine pesticides from water. The optimized parameters were employed to perform extraction of the pesticides from natural waters.

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References

  1. B. A. Tomkins, R. Merriweather, R. A. Jenkins, C. K. Bayne, J. Assoc. Off. Anal. Chem. Int.75, 1091 (1992).

    CAS  Google Scholar 

  2. C. Markell, D. F. Hagen, V. A. Bunnelle, LC-GC9, 332 (1993).

    Google Scholar 

  3. M. C. Hennion, Trends in Anal. Chem.10, 317 (1991).

    Article  CAS  Google Scholar 

  4. G. Manes, Y. Pico, J. C. Molto, G. Font, J. High Res. Chromatogr.13, 843 (1990).

    Article  CAS  Google Scholar 

  5. G. Rene van der Hoff, S. M. Gort, R. A. Baumann, P. V. Zoonen, U. A. Th. Brinkman, J. High Res. Chromatogr.14, 465 (1991).

    Article  Google Scholar 

  6. L. Torreti, A. Simonella, A. Dossena, E. Torreti, J. High Res. Chromatogr.15, 99 (1992).

    Article  CAS  Google Scholar 

  7. W. G. Lan, M. K. Wong, N. Chen, Y. M. Sin, Analyst119, 1659 (1994).

    Article  CAS  Google Scholar 

  8. W. G. Lan, M. K. Wong, N. Chen, Y. M. Sin, Analyst119, 1669 (1994).

    Article  CAS  Google Scholar 

  9. H. B. Wan, W. G. Lan, M. K. Wong, C. Y. Mok, Anal. Chim. Acta289, 371 (1994).

    Article  CAS  Google Scholar 

  10. H. B. Wan, W. G. Lan, M. K. Wong, C. Y. Mok, Y. H. Poh, J. Chromatogr.677, 255 (1994).

    Article  CAS  Google Scholar 

  11. W. G. Lan, M. K. Wong, N. Chen, Y. M. Sin, Talanta41, 1917 (1994).

    Article  CAS  Google Scholar 

  12. W. G. Lan, K. K. Chee, M. K. Wong, Y. M. Sin, Analyst120, 273 (1995).

    Article  CAS  Google Scholar 

  13. W. G. Lan, K. K. Chee, M. K. Wong, H. K. Lee, Analyst120, 281 (1995).

    Article  CAS  Google Scholar 

  14. S. N. Deming, J. M. Palasota, J. Lee, L. Sun, J. Chromatogr.485, 3 (1989).

    Article  Google Scholar 

  15. Y. Hu, D. L. Massart, J. Chromatogr.485, 311 (1989).

    Article  CAS  Google Scholar 

  16. P. J. Oles, J. Assoc. Off. Anal. Chem. Int.76, 615 (1993).

    CAS  Google Scholar 

  17. P. M. J. Coenegracht, A. K. Smlide, H. J. Metting, D. A. Doornbos, J. Chromatogr.485, 15 (1989).

    Article  Google Scholar 

  18. W. E. Johnson, N. J. Fendinger, J. R. Plimer, Anal. Chem.63, 1510, (1991).

    Article  CAS  Google Scholar 

  19. J. Beltran, F. J. Lopez, F. Hernandez, Anal. Chim. Acta283, 97 (1993).

    Article  Google Scholar 

  20. A. G. Kelly, I. Cruz, D. E. Wells, Anal. Chim. Acta276, 3 (1993).

    Article  CAS  Google Scholar 

  21. I. Cruz, D. E. Wells, I. L. Marr, Anal. Chim. Acta283, 280 (1993).

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Department of Chemistry, National University of Singapore, 0511, Kent Ridge, Republic of Singapore

    K. K. Chee, M. K. Wong & H. K. Lee

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  1. K. K. Chee
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  2. M. K. Wong
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  3. H. K. Lee
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Chee, K.K., Wong, M.K. & Lee, H.K. Optimization by orthogonal array design of solid phase extraction of organochlorine pesticides from water. Chromatographia 41, 191–196 (1995). https://doi.org/10.1007/BF02688024

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  • DOI: https://doi.org/10.1007/BF02688024

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