Summary
Phenylamino-propanediols were analysed by capillary gas chromatography as various derivatives. Trimethylsilyl and methylboronic acid derivatives were detected with a FID. The trifluoroacetyl derivatives were analysed using an ECD. The structure of the derivatives was confirmed by GC-MS.
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References
Hungarian patent: 174–125.
Th. Walle, J. Pharm. Sci.63, 1885 (1974).
M. D. Rawlins, P. Collste, M. Frisk-Holmberg, M. Lind, J. Östman, F. Sjöqvist, Europ. J. Clin. Pharmacol.7, 33 (1974).
Kenji Kawahara, Tatsuya Ofuji, J. Chromatogr.168, 266 (1979).
M. Ervik, K. Kylberg-Hanssen, P.P. Lagerstrom, J. Chromatogr.182, 341 (1980).
A. Sioufi, F. Leroux, N. Sandrenan, J. Chromatogr.272, 103 (1983).
K. Blau, G. S. King (eds.), Handbook of Derivatives for Gas Chromatography, Heyden, London, 1977.
C. F. Poole, S. Singhawangcha, A. Zlatkis, J. Chromatogr.186, 307 (1979).
C. F. Poole, L. Johansson, J. Vessman, J. Chromatogr.194, 365 (1980).
E. Sherwood, C. F. Poole, Wen-Fa Sye, A. Zlatkis, J. Chromatogr.205, 297 (1981).
Gy. Vigh, O. Etler, J. High Res. Chrom. and Chrom. Comm.7, 374 (1984).
E. Wetzel, Th. Kuster, J. Chromatogr.268, 177 (1983).
C. A. Clemons, A. P. Altshuller, Anal. Chem.38, 133 (1966).
E. D. Morgan, C. F. Poole, J. Chromatogr.89, 225 (1974).
G. M. Anthony, C. J. W. Brooks, I. MacLean, I. Sangster, J. Chromatogr. Sci.7, 623 (1969).
C. J. W. Brooks, I. MacLean, J. Chromatogr. Sci.9, 18 (1971).
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Lakszner, K., Szepesy, L. & Vida, L. Comparison and evaluation of derivatization methods for gas chromatographic determination of various propane-diols. Chromatographia 19, 304–309 (1984). https://doi.org/10.1007/BF02687760
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DOI: https://doi.org/10.1007/BF02687760