Summary
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1.
Batches of soybean oil weighing up to 54 pounds have been chlorinated withtert-butyl hypochlorite in conventional pilot-plant equipment.
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2.
The chlorinated oil was dehydrochlorinated in an all-glass apparatus designed for continuous operation. Excellent results were obtained when chlorinated oil was passed through this apparatus at a rate of 1.5 liters per hour.
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3.
The properties of the dehydrochlorinated oil were equivalent to those of oils previously obtained by laboratory procedures.
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References
Chattaway, F. D., and Backeberg, O. G., J. Chem. Soc.,1923, 2999–3003.
Teeter, H. M., Bachmann, R. C., Bell, E. W., and Cowan, J. C., Ind. Eng. Chem.,41, 849–52 (1949).
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One of the laboratories of the Bureau of Agricultural and Industrial Chemistry, Agricultural Research Administration, U. S. Department of Agriculture.
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Bell, E.W., Teeter, H.M. Reactions of tertiary butyl hypochlorite with vegetable oils and their derivatives. III. Chlorination of soybean oil in the pilot plant. J Am Oil Chem Soc 27, 102–105 (1950). https://doi.org/10.1007/BF02634400
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DOI: https://doi.org/10.1007/BF02634400