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Substituted calix[n]arenes. Synthesis ofp-isopropylcalix[4]arene and the structure of its benzene clathrate

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Abstract

p-Isopropylcalix[4]arens was synthesized by alkylation of unsubstituted calix[4]arene in the presence of ferric chloride hexahydrate. The structure of the compound and its benzene clathrate was established by NMR spectroscopy and X-ray diffraction analysis.

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References

  1. J. Vicens, H. T. Pilot, D. Gamet, et al.,C. R. Acad. Sci. Paris,302, No. 2, 15 (1986).

    CAS  Google Scholar 

  2. A. M. Yuldashev, S. U. Ubaidullaeva, and M. A. Ishmukhamedov,Uzb. Khim. Zh., No. 3, 31 (1994).

    Google Scholar 

  3. A. M. Yuldashev, S. U. Ubaidullaeva, and M. A. Ishmukhamedov, —ibid., No. 4, 47 (1994).

    Google Scholar 

  4. G. M. Sheldrick,SHELXS-86. Program for Solution of Crystal Structures, Göttingen University (1986).

  5. G. M. Sheldrick,SHELX-76. Program for Crystal Structure Determination, Cambridge University (1976).

  6. G. D. Andreetti, R. Ungaro, and A. Pochini,J. Chem. Soc., Chem. Commun., 1005 (1979).

  7. R. Ungaro, A. Pochini, G. D. Andreetti, and V. Sangermono,J. Chem. Soc., Perkin Trans., No 2, 1979–1985 (1985).

    Google Scholar 

  8. R. Ungaro, A. Pochini, G. D. Andreetti, and P. Domiano, —ibid.,. 197–201.

    Google Scholar 

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Tashkent State University. A. S. Sadykov Institute of Bioorganic Chemistry, Academy of Sciences, Uzbekistan. Translated fromZhurnal Strukturnoi Khimii, Vol. 37, No. 3, pp. 539–543, May–June, 1996.

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Yuldashev, A.M., Ibragimov, B.T., Talipov, S.A. et al. Substituted calix[n]arenes. Synthesis ofp-isopropylcalix[4]arene and the structure of its benzene clathrate. J Struct Chem 37, 470–473 (1996). https://doi.org/10.1007/BF02578603

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  • DOI: https://doi.org/10.1007/BF02578603

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