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Thermal properties and morphology of crystal in nylon 1010 formed isothermally at melting peak temperature

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Abstract

Thermal properties and morphology of crystal in NYLON 1010 formed isothermally at melting peak temperature were studied by using DSC, TEM and ED. It turns out that the crystal on the time scale of the DSC experiment is stable, which is not transformed from the crystal with low melting point. Its electron diffraction pattern shows symmetrical and clear electron diffraction spots of single crystal and is proved to be the electron diffraction pattern of single crystal by means of index with parameters of unit cell of Nylon 1010

Zusammenfassung

Mittels DSC, TEM und ED wurden die thermischen Eigneschaften und die Kristallmorphologie in NYLON 1010 untersucht, welches isotherm bei der Schmelzpeak-temperatur gebildet wurde. Es zeigt sich, daß sich der Kristall in der Zeitskala des DSC-Experimentes stabil erweist, welcher nicht aus dem Kristall mit niedrigem Schmelzpunkt umgewandelt wird. Die Elektronenbeugungsbilder zeigen eine symmetrische und klare Elektronenbeugung von Einkristallen und erweisen sich als Elektronenbeugungsbild eines Einkristalles mit Hilfe von Indizes mit den Parametern der Elementarzelle von Nylon 1010.

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Shuren, F., Guanghua, Z., Qun, T. et al. Thermal properties and morphology of crystal in nylon 1010 formed isothermally at melting peak temperature. Journal of Thermal Analysis 40, 689–695 (1993). https://doi.org/10.1007/BF02546640

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  • DOI: https://doi.org/10.1007/BF02546640

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