Abstract
Diazelains can be quantitatively removed from mixtures of di- and monoazelains by treatment in diethyl ether with saturated aqueous sodium bicarbonate under specified conditions. The total monoazelains produced by oxidation of GS3nil fats of C16-C18 acid type can be isolated quantitatively for further examination by applying this procedure to the insoluble azelaoglycerides. Similar treatment of the insoluble azelaoglycerides from GS3 positive fats will give a mixture of GS3 and GS2A in the bicarbonate insoluble fraction. The GS3 can be accurately estimated from the analysis of the latter by already available procedures.
References
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Kartha, A.R.S. Quantitative separation of diazelaoglycerides from insoluble azelaoglycerides and its applications in glyceride structure studies. J Am Oil Chem Soc 46, 632–633 (1969). https://doi.org/10.1007/BF02544985
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DOI: https://doi.org/10.1007/BF02544985