Abstract
A method for preparation of uranium-and plutonium-measuring probes for α-spectrometry is described. The method is based on electrodeposition from isopropanol and especially from ethanol and methanol solution. It was shown that a definite addition of a little amount of water lead to an increasing of the deposition speed by ethanol and methanol. It is possible to reach in ethanol a 100% deposition grade after an electrolysis time of 3 minutes for uranium and 30 minutes for plutonium with voltages of 150–200 V.
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Gruner, W., Beutmann, A. Elektrolytische Uran-und Plutonium-Präparateherstellung für die Alpha-Spektrometrie aus Organischen Lösungen. J. Radioanal. Chem. 58, 89–94 (1980). https://doi.org/10.1007/BF02533775
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DOI: https://doi.org/10.1007/BF02533775