Lipids

, Volume 4, Issue 5, pp 327–330 | Cite as

The quantitative production of aldehydes from O-alk-1-enyl glycerols

  • Robert E. Anderson
  • Ronald D. Garrett
  • M. L. Blank
  • Fred Snyder
Article

Abstract

The quantitative recovery and structural alterations of aldehydes liberated from O-alk-1-enyl glycerols on thin layer chromatographic layers have been evaluated by using14C-labeled fatty aldehydes and chromatography. The results led to the development of a quantitative procedure for isolating the aldehydes produced from O-alk-1-enyl glycerols by shaking an ethereal solution of the ether-linked lipids with concentrated hydrochloric acid. The procedure is rapid and silicic acid does not interfere.

Keywords

Aldehyde Silicic Acid Preparative Thin Layer Chromatography Isopropylidene Lithium Aluminum Hydride 

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Copyright information

© American Oil Chemists’ Society 1969

Authors and Affiliations

  • Robert E. Anderson
    • 1
  • Ronald D. Garrett
    • 1
  • M. L. Blank
    • 1
  • Fred Snyder
    • 1
  1. 1.The Medical Division, Lipid Research LaboratoriesOak Ridge Associated UniversitiesOak Ridge

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