The quantitative production of aldehydes from O-alk-1-enyl glycerols
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The quantitative recovery and structural alterations of aldehydes liberated from O-alk-1-enyl glycerols on thin layer chromatographic layers have been evaluated by using14C-labeled fatty aldehydes and chromatography. The results led to the development of a quantitative procedure for isolating the aldehydes produced from O-alk-1-enyl glycerols by shaking an ethereal solution of the ether-linked lipids with concentrated hydrochloric acid. The procedure is rapid and silicic acid does not interfere.
KeywordsAldehyde Silicic Acid Preparative Thin Layer Chromatography Isopropylidene Lithium Aluminum Hydride
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- 1.Schmid, H. H. O. and H. K. Mangold, Biochim. Biophys. Acta125, 182 (1966).Google Scholar
- 2.Schmid, H. H. O. and H. K. Mangold, Biochem. Z.346, 13 (1966).Google Scholar
- 6.Wood, R. and F. Snyder, Lipids3, 129 (1968).Google Scholar
- 7.Mahadevan, V., F. Phillips and W. O. Lundberg, Ibid.1, 183 (1966).Google Scholar
- 8.Jangaard, P. M. and R. G. Ackman, J. Fisheries Res. Board Can.18, 865 (1961).Google Scholar
- 10.Wood, R., Lipids2, 199 (1967).Google Scholar
- 13.Wood, R., and R. Harlow, USAEC Report ORAU 106,1968, 144.Google Scholar