Abstract
Specific advantages with Particle Induced X-Ray Emission are: its (1) multielemental capability, especially when combined with nuclear techniques for lighter elements, (2) speed, (3) low detection limits for small samples and (4) accuracy. To make full use of these advantages, analytical parameters have to be chosen optimally and the facility to be carefully designed. This paper describes an experimental facility constructed to permit continuous development work to optimize the analytical conditions and to allow the gradual implementation of automatic control. Emphasis is also put on the simultaneous use of proton induced gamma rays from fluorine. The features and the performance of the set-up including its accuracy, precision and experimental detection limits are reported.
Similar content being viewed by others
References
T. B. JOHANSSON, R. AKSELSSON, S. A. E. JOHANSSON, Nucl. Instr. Meth., 84 (1970) 141.
Proc. Int. Conf. on Particle Induced X-Ray Emission and its Anal. Applic., Nucl. Instr. Meth., 142 (1977).
Proc. Sec. Int. Conf. on Particle Induced X-Ray Emission and its Analytical Application, Nucl., Instr. Meth., 181 (1981).
J. W. NELSON, D. L. MEINERT, Adv. X-Ray Anal., 18 (1975) 598.
T. A. CAHILL, in New Uses of Ion Accelerator, J. F. ZIEGLER (Ed.) Plenum Press (1975) p. 1.
R. D. LEAR, H. A. VAN RINSVELT, W. R. ADAMS, Adv. X-Ray Anal., 19 (1976) 521.
R. B. BOULTON, G. T. EWAN, Anal. Chem., 49 (1977) 1297.
L.-E. CARLSSON, K. R. AKSELSSON, Nucl. Instr. Meth., 181 (1981) 531.
K. G. MALMQVIST, G. I. JOHANSSON, M. BOHGARD, K. R. AKSELSSON, Nucl. Instr. Meth., 181 (1981) 465.
E. MÖLLER, N. STARFELT, Nucl. Instr. Meth., 50 (1967) 225.
J. W. MANDLER, R. B. MOLER, E. RAISEN, K. S. RAJAN, Thin Solid Films, 19 (1973) 165.
K. ISHI, S. MORITA, H. TAWARA, Phys. Rev. A, 13 (1976) 131.
M. AHLBERG, G. JOHANSSON, K. MALMQVIST, Nucl. Instr. Meth., 131 (1975) 377.
K. G. MALMQVIST, E. KARLSSON, K. R. AKSELSSON, Nucl. Instr. Meth., 192 (1982) 523.
H. C. KAUFMANN, K. R. AKSELSSON, W. J. COURTNEY, Nucl. Instr. Meth., 142 (1977) 251.
G. I. JOHANSSON, accepted for publication in X-Ray Spectrometry.
G. I. JOHANSSON, J. PALLON, K. G. MALMQVIST, K. R. AKSELSSON, Nucl. Instr. Meth., 181 (1981) 81.
J. A. HEAGNEY, J. S. HEAGNEY, Nucl. Instr. Meth., 167 (1979) 137.
T. A. THORNTON, J. N. ANNO, J. Appl. Phys., 48 (1977) 1718.
R. AKSELSSON, T. B. JOHANSSON, Nucl. Instr. Meth., 91 (1971) 663.
L. MEYER, Phys. Stat. Sol., 44 (1971) 253.
R. NOBILING, Y. CIVELEKOGLU, P. POVH, D. SCHWALM, K. TRAXEL, Nucl. Instr. Meth., 130 (1975) 325.
F. FOLKMANN, J. Phys. E, 8 (1975) 429.
F. S. GOULDING, J. M. JACLEVIC, B. V. JARRETT, D. A. LANDIS, Adv. X-Ray Anal., 15 (1972) 470.
R. HELLBORG, L. ASK, Physica Scripta, 6 (1972) 47.
H. B. WILLARD, J. K. BAIR, J. D. KINGTON, T. M. HAHN, C. W. SNYDER F. P. GREEN, Phys. Rev., 85 (1952) 849.
I. GOLICHEFF, M. LOEUILLET, Ch. ENGELMANN, J. Radioanal Chem., 12 (1972) 233.
S. A. E. JOHANSSON, T. B. JOHANSSON, Nucl. Instr. Meth., 137 (1976) 473.
A. W. HERMAN, L. A. McNELLES, J. L. CAMPBELL, Int. J. Appl. Radiat. Isot., 24 (1973) 677.
B. RAITH, M. ROTH, K. GÖLLNER, B. GONSIOR, H. OSTERMANN, C. O. UHLHORN, Nucl. Instr. Meth., 142 (1977) 39.
L. C. NORTHCLIFFE, R. F. SCHILLING, Nucl. Data Tables, A7 (1970) 233.
P. L. BAILEY, Analysis With Ion-Selective Electrode, Heyden, London, 1976.
M. PANTUČEK, Am. Ind. Hyg. Ass. J., 32 (1971) 687.
Except for the authors, the Lund PIXE group comprises the following persons: M. BOHGARD, L.-E. CARLSSON, H.-C. HANSSON, E.-M. JOHANSSON, S. A. E. JOHANSSON, H. LANNEFORS, LI HUNG-KOU, J. PALLON.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Malmqvist, K.G., Johansson, G.I. & Akselsson, K.R. A facility for multielemental analysis by PIXE and the19F(p, αγ)16O reaction. J. Radioanal. Chem. 74, 125–147 (1982). https://doi.org/10.1007/BF02520366
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF02520366