Skip to main content
Log in

Determination of isotopic composition and concentration of uranium, plutonium and neodymium by mass-spectrometric isotope dilution in the irradiated fuel of the Czechoslovak atomic power station A-1

  • Analytical Chemistry of Nuclear Fuel Cycle
  • Published:
Journal of Radioanalytical Chemistry Aims and scope Submit manuscript

Abstract

Determination of the isotopic composition and concentration of uranium, plutonium and neodymium by mass-spectrometric isotope dilution is described. Isotopes233U,242Pu and150Nd were used as spikes. Isotopic composition was measured with a Varian-TH 5 mass spectrometer. Optimum amounts loaded onto the filament were 2–5 μg U, ∼0.1 μg Pu and <0.1 μg Nd. The accuracy and reproducibility of the isotopic ratio and concentration measurements were evaluated.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. V. BULOVIČ, J. KRTIL, F. SUS, Z. MAKSIMOVIČ, E. KLOSOVÁ, J. Radioanal. Chem., 51 (1979) 153.

    Google Scholar 

  2. E. KLOSOVÁ, V. KNOBLOCH, J. KRTIL, V. KUVIK, M. KŘIVÁNEK, J. MORAVEC. V. SPĚVÁČKOVÁ, F. SUS, V. ŠÁRA. Report ÚJV 4018-CH, M. May 1977.

  3. F. SUS, E. KLOSOVÁ, E. ŠTĚPÁNKOVÁ, V. FRAŇKOVÁ, Radiokhimiya (in press).

  4. F. SUS, E. KLOSOVÁ, E. ŠTEPÁNKOVÁ, V. FRANŇKOVÁ, Mass-spectrometric determination of burn-up of nuclear fuel with the aid of148Nd. Symp. on Research in the field of reprocessing of irradiated fuel, 28 March–1 April 1977, Karlovy Vary, ČSSR, Paper No KV 77/13.

  5. J. E. REIN, C. F. METZ, Proc. IAEA Panel Analytical Chemistry of Nuclear Fuel, IAEA, Vienna 1972, p. 97.

  6. L. KOCH, Radiochim. Acta, 12 (1969) 160.

    CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Sus, F., Krtil, J., Bulovič, V. et al. Determination of isotopic composition and concentration of uranium, plutonium and neodymium by mass-spectrometric isotope dilution in the irradiated fuel of the Czechoslovak atomic power station A-1. J. Radioanal. Chem. 51, 143–151 (1979). https://doi.org/10.1007/BF02519932

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02519932

Keywords

Navigation