Skip to main content
Log in

Determination of 22 elements in geological samples by instrumental neutron activation analysis

  • Physical Methods Section
  • Published:
Journal of Radioanalytical Chemistry Aims and scope Submit manuscript

Abstract

An instrumental neutron activation analysis (INAA) method has been developed for multi-element determination in geological samples. The INAA method consists of irradiation of samples for 90 sec at a flux of 1.0·1012 n·cm−2·sec−1 and determination of 12 elements by using their short-lived nuclides. Samples have been re-irradiated for 3 hrs for measuring concentrations of another 10 elements. Precision and accuracy of the INAA method have been evaluated by analysing samples and USGS standard reference materials. Precision and accuracy are within±15% and ±10%, respectively.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. O. B. MICHELSEN, E. STEINNES, Proc. Modern Trends in Activation Analysis, Gaithersburg, MD, USA 1965, p. 315.

  2. J. C. COBB, Anal. Chem., 39 (1967) 127.

    Article  CAS  Google Scholar 

  3. G. E. GORDON, K. RANDLE, G. C. GOLES, J. B. CORLISS, M. H. BEESON, S. S. OXLEY, Geochim. Cosmochim. Acta, 32 (1968) 369.

    Article  CAS  Google Scholar 

  4. Z. RANDA, J. BENADA, J. KUNCIR, M. VOBECKY, J. FRANA, J. Radioanal. Chem., 11 (1972) 305.

    Article  CAS  Google Scholar 

  5. M. MANTEL, S. AMIEL, J. Radioanal. Chem., 16 (1973) 127.

    Article  CAS  Google Scholar 

  6. M. ELLINGER, M. JANGHORBANI, K. STARKE, J. Radioanal. Chem., 32 (1976) 473.

    CAS  Google Scholar 

  7. R. A. NADKARNI, Radiochem. Radioanal. Letters, 25 (1976) 159.

    CAS  Google Scholar 

  8. J. J. ROWE, E. STEINNES, J. Res. U. S. Geol. Survey, 5 (1977) 397.

    CAS  Google Scholar 

  9. G. H. MORRISON, J. T. GERARD, A. TRAVESI, R. L. CURRIE, S. F. PETERSON, N. M. POTTER, Anal. Chem., 41 (1969) 1633.

    Article  CAS  Google Scholar 

  10. J. C. LAUL, D. R. CASE, M. WECHTER, F. SCHMIDT-BLEEK, M. E. LIPSCHUTZ, J. Radioanal. Chem., 4 (1970) 241.

    Article  CAS  Google Scholar 

  11. A. O. BRUNFELT, I. ROELANDTS, E. STEINNES, Analyst, 99 (1974) 277.

    Article  CAS  Google Scholar 

  12. P. VOLDET, W. HAERDL, Anal. Chim. Acta, 87 (1976) 227.

    Article  CAS  Google Scholar 

  13. G. R. REDDY, D. R. PANT, B. L. RAO, M. SANKAR DAS, J. Radioanal. Chem., 33 (1976) 39.

    CAS  Google Scholar 

  14. G. R. REDDY, B. L. RAO, D. R. PANT, Radiochem. Radioanal. Letters, 26 (1976) 129.

    CAS  Google Scholar 

  15. Z. RANDA, Radiochem. Radioanal. Letters, 24 (1976) 177.

    CAS  Google Scholar 

  16. G. M. KOLESOV, J. Radioanal. Chem., 30 (1976) 553.

    CAS  Google Scholar 

  17. R. J. N. BRITS, G. J. GREEFF, Microchim. Acta, 1 (1977) 105.

    Article  CAS  Google Scholar 

  18. D. I. LEYPUNSKAYA, V. I. DRYNKIN, B. V. BELENKY, M. A. KOLOMITSEV, V. YU. DUNDUA, N. V. PACHULIA, J. Radioanal. Chem., 26 (1975) 293.

    Google Scholar 

  19. I. M. H. PAGDEN, G. J. PEARSON, J. M. BEWERS, J. Radioanal. Chem., 8 (1971) 127, 8 (1971) 373., 9 (1971) 101.

    Article  CAS  Google Scholar 

  20. A. CHATTOPADHYAY, J. Radioanal. Chem., 37 (1977) 785.

    CAS  Google Scholar 

  21. D. E. Ryan, D. C. Stuart, A. Chattopadhyay, Anal. Chim. Acta, 100 (1978) (in press).

  22. S. T. KOSIEWICZ, P. J. SCHOMBERG, L. A. HASKIN, J. Radioanal. Chem., 20 (1974) 619.

    Article  CAS  Google Scholar 

  23. F. J. FLANAGAN (Ed.), Descriptions and Analyses of Eight New USGS Rock Standards, Geological Survey Professional Paper 840, U. S. Govt. Printing Office, Washington, D. C., 1976, p. 192.

    Google Scholar 

  24. A. KATZ, L. GROSSMAN, Descriptions and Analyses of Eight New USGS Rock Standards, Geological Survey Professional Paper 840, U.S. Govt. Printing Office, Washington, D. C., 1976, p. 49.

    Google Scholar 

  25. J. R. DE LAETER, R. DATE, I. D. ABERCROMBIE, Descriptions and Analyses of Eight New USGS Rock Standards, Geological Survey Professional Paper 840, U. S. Govt. Printing Office, Washington, D. C., 1976, p. 41.

    Google Scholar 

  26. B. P. FABBI, L. F. ESPOS, Descriptions and Analyses of Eight New USGS Rock Standards, Geological Survey Professional Paper 840, U. S. Govt. Printing Office, Washington, D. C., 1976, p. 89.

    Google Scholar 

  27. I. B. BRENNER, A. HAREL, Descriptions and Analyses of Eight New USGS Rock Standards, Geological Survey Professional Paper 840, U. S. Govt. Printing Office, Washington, D. C., 1976, p. 95.

    Google Scholar 

  28. F. G. WALTHALL, A. F. DORRZAPF, Jr., F. J. FLANAGAN, Descriptions and Analyses of Eight New USGS Rock Standards, Geological Survey Professional Paper 840, U. S. Govt. Printing Office, Washington, D. C., 1976, p. 99.

    Google Scholar 

  29. J. A. THOMAS, W. MOUNTJOY, C. HUFFMAN, Jr., Descriptions and Analyses of Eight New USGS Rock Standards, Geological Survey Professional Paper 840, U.S. Govt. Printing Office, Washington, D. C., 1976, p. 119.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Chattopadhyay, A., Katz, S.A. Determination of 22 elements in geological samples by instrumental neutron activation analysis. J. Radioanal. Chem. 46, 321–332 (1978). https://doi.org/10.1007/BF02519898

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02519898

Keywords

Navigation