Skip to main content
Log in

Reactor-detector calibration for routine instrumental neutron activation analysis of geological materials

  • Physical Methods Section
  • Published:
Journal of radioanalytical chemistry Aims and scope Submit manuscript

Abstract

A reactor-detector combination has been calibrated for routine determination of trace elements by instrumental neutron activation analysis using the semi-absolute method with flux corrections. The reproducibility of the calibration constants is studied using the standard rock AGV-1 for the activities140La,141Ce,153Sm,160Tb,152Eu,175Yb,177Lu,131Ba,60Co,51Cr,134Cs,181Hf,233Pa,46Sc, and182Ta. The results show that a calibration reproducibility with a relative precision of better than 5% can be achieved in many of the cases without any special precautions. To study the applicability of the calibration constants, concentrations of the corresponding elements have been determined in standard rocks, G-2, W-1 and GSP-1 and are compared with the recommended values.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. G. E. GORDON, K. RANDLE, G. G. GOLES, J. B. CORLISS, M. H. BEESON, S. S. OXLEY, Geochim. Cosmochim. Acta, 32 (1968) 369.

    Article  CAS  Google Scholar 

  2. J. KUNCIR, J. BENADA, Z. RANDA, M. VOBECKY, J. Radioanal. Chem., 5 (1970) 369.

    Article  CAS  Google Scholar 

  3. J. W. JACOBS, R. L. KOROTEV, D. P. BLANCHARD, L. A. HASKIN, J. Radional Chem., 40 (1977) 93.

    Article  CAS  Google Scholar 

  4. A. CHATTOPADHYAY, S. A. KATZ, J. Radioanal. Chem., 46 (1978) 321.

    Article  CAS  Google Scholar 

  5. D. E. RYAN, D. C. STUART, A. CHATTOPADHYAY, Anal. Chim. Acta, 100 (1978) 87.

    Article  CAS  Google Scholar 

  6. P. SCHRAMEL, W. SCHMOLKE, H. MUNTAU, J. Radioanal. Chem., 50 (1979) 179.

    Article  CAS  Google Scholar 

  7. F. J. FLANAGAN, Geochim. Cosmochim. Acta, 37 (1973) 1189.

    Article  CAS  Google Scholar 

  8. P. ILA, P. JAGAM, G. K. MUECKE, Third European Conference on Analytical Chemistry, Euroanalysis III, Dublin, Ireland, 1978, p. 193.

  9. C. BERGERIOUX, G. KENNEDY, L. ZIKOVSKY, J. Radioanal. Chem., 50 (1979) 229.

    Article  CAS  Google Scholar 

  10. J. T. ROUTTI, S. G. PRUSSIN, Nucl. Instr. Meth., 72 (1965) 125; J. T. ROUTTI, UCRL-19452, 1969.

    Article  Google Scholar 

  11. S. ABBEY, Studies in “Standard Samples” for use in the general analysis of silicate rocks and minerals, Part 5: 1977 edition of “Usable” values, Geological Survey of Canada Paper 77-34.

  12. S. ABBEY, Geostand. News Lett., 2 (1978) 137.

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Ila, P., Jagam, P. & Muecke, G.K. Reactor-detector calibration for routine instrumental neutron activation analysis of geological materials. J. Radioanal. Chem. 57, 147–155 (1980). https://doi.org/10.1007/BF02519874

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02519874

Keywords

Navigation