Skip to main content
Log in

Determination of sulfur and moisture in coal using capture gamma-rays

  • Physical Methods Section
  • Published:
Journal of Radioanalytical Chemistry Aims and scope Submit manuscript

Abstract

Samples of coal weighing approximately 200 g placed in a collimated beam of neutrons from the thermal column of the Ames Laboratory Research Reactor produce capture gamma-rays which can be used for the determination of sulfur in the presence of iron, a potential source of interference. Spectra from NaI(Tl) detectors were used with the help of Ge(Li) spectra to locate interferences. Corrections for iron interference was made by the use of a higher energy iron peak. A linear relation was found between the area of the hydrogen capture peak at 2.23 MeV and the amount of water added to coal.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. S. P. BABU (Ed.), Trace Elements in Fuel, Advances in Chemistry Series No. 141, American Chemical Society, Washington, DC, 1975.

    Google Scholar 

  2. N. C. RASMUSSEN, Y. HUKAI, Trans. Am. Nuc. Soc., 10 (1967) 29.

    Google Scholar 

  3. N. C. RASMUSSEN, Analysis Instrum., 7 (1969) 186.

    CAS  Google Scholar 

  4. N. C. RASMUSSEN, Trans. Am. Nuc. Soc., 14 (1971) 931.

    Google Scholar 

  5. D. R. PARSIGNAULT, H. H. WILSON, R. MINESKI, In Neutron Sources and Applications, Proc. Amer. Nucl. Soc. Meeting April 19–21, 1971, Augusta, GA, AEC Report CONF 710402, Vol. III Session IV, p. 40.

  6. A. R. POURAGHABAGHER, A. E. PROFIO, Anal. Chem., 46 (1974) 1223.

    Article  CAS  Google Scholar 

  7. R. F. STEWART, A. W. HALL, J. W. MARTIN, W. L. FARRIOR, A. M. POSTON, Nuclear Meter for Monitoring the Sulfur Content of Coal Streams, U.S. Bureau of Mines Technical Progress Report 74, Jan. 1974.

  8. A. W. HALL, J. W. MARTIN, R. F. STEWART, A. M. POSTON, Precision Tests of Neutron Sulfur Meter in Coal Preparation Plant, U.S. Bureau of Mines Report of Investigations 8038, 1975.

  9. G. F. FASCHING, G. H. PATTON, U. S. Pat. 3,868,509, Feb. 25, 1975.

  10. A. W. HALL, J. L. KONCHESKY, R. F. STEWART, Continuous Monitoring of Coal by a Neutron Moisture Meter, U. S. Bureau of Mines Report of Investigations 7807, 1973.

  11. V. J. ORPHAN et al., Line and Continuum Gamma-Ray Yields from Thermal Neutron Capture in 75 Elements, Report AD 717639, USNTIS, Springfield, Va. 1970.

  12. D. DUFFEY, A. ELKADY, F. E. SENFTLE, Nucl. Instr. Methods, 80 (1970) 149.

    Article  CAS  Google Scholar 

  13. F. E. SENFTLE, H. D. MOORE, D. B. LEEP, A. ELKADY, D. DUFFEY, Nucl. Instr. Methods, 93 (1971) 425.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Fay, D.A., Pazirandeh, A., Struss, R.G. et al. Determination of sulfur and moisture in coal using capture gamma-rays. J. Radioanal. Chem. 43, 263–274 (1978). https://doi.org/10.1007/BF02519464

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02519464

Keywords

Navigation