Abstract
Errors arising from solubility losses and co-precipitation in the gravimetric determination of fluoride by precipitation of calcium fluoride by classical and homogeneous methods have been investigated by radiometric techniques. It is shown that co-precipitation of chloride is the larger source of error and least in the homogeneous method. Distribution of chloride in the calcium fluoride precipitate is shown to follow the Doerner-Hoskins distribution law.
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Tcholakova, I., Whitley, J.E. A radiometric investigation of the precipitation of calcium fluoride. J. Radioanal. Chem. 2, 409–414 (1969). https://doi.org/10.1007/BF02518468
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DOI: https://doi.org/10.1007/BF02518468