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Journal of Radioanalytical Chemistry

, Volume 16, Issue 1, pp 105–114 | Cite as

Neutron activation determination of lanthanum in praseodymium oxide near the detection limit. Comparison of various procedures

  • R. Dybczyński
  • S. Sterliński
  • C. Golian
Thermal Neutron Activation and Radiochemistry

Abstract

Trace amounts of lanthanum in spectrally pure praseodymium oxide have been determined by four independent methods: (1) non-destructive Ge(Li) spectrometry, (2) spectrometry of slow γ-γ coincidences, (3) radiochemical separation of140La from macro amounts of142Pr and other interfering activities (mainly192,194Ir and152,154Eu) with∼100% yield, by several ion-exchange steps followed by NaI(Tl) spectrometry, (4) method of standard additions using the same procedure as in method (3). Near the detection limit only the two last methods gave accurate results.

Keywords

Lanthanum Neutron Activation Iridium Radiochemical Separation Background Count Rate 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Copyright information

© Akadémiai Kiadó 1973

Authors and Affiliations

  • R. Dybczyński
    • 1
  • S. Sterliński
    • 1
  • C. Golian
    • 1
  1. 1.Department of Analytical ChemistryInstitute of Nuclear ResearchWarsaw(Poland)

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