Skip to main content
Log in

Study on the applicability of the integral counting method for the determination of226Ra in various sample forms using a liquid scintillation counter

  • Published:
Journal of Radioanalytical Chemistry Aims and scope Submit manuscript

Abstract

A new counting method was developed to determine226Ra in environmental samples by separating the equilibrated222Rn into a liquid scintillator. The integral counting method, which was originally developed for isolated individual radionuclides, was extended to the mixture of222Rn and its daughters in equilibrium. The optimum measurement conditions were established by examining the energy spectrum, counting time and quenching effect. An absolute counting was practiced by extrapolating the integral counting rate-bias voltage curve with the highest gain to zero bias. The detection limit thus obtained was 3 to 4·10−13 Ci.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. H. W. KRANER, G. L. SCHROEDER, A. R. LEWIS, R. D. EVANS, Rev. Sci. Instr., 35 (1964) 1259.

    Article  CAS  Google Scholar 

  2. K. KURODA, Y. YOKOYAMA, Bull. Chem. Soc. Japan, 21 (1948) 52.

    Article  CAS  Google Scholar 

  3. J. E. PEARSON, G. E. JONES, Tellus, 18 (1966) 655.

    Article  CAS  Google Scholar 

  4. M. L. CURTISS, H. L. ROOK, Anal. Chem., 36 (1964) 2047.

    Article  Google Scholar 

  5. J. F. EICHELBERGER, G. R. GROVE, L. V. JONES, USAEC Rept., MLM-1250, 1965.

  6. L. A. BAILLIE, Intern. J. Appl. Radiation Isotopes, 8 (1960) 1.

    Article  CAS  Google Scholar 

  7. G. A. BRUNO, J. E. CHRISTIAN, Anal. Chem., 33 (1961) 650.

    Article  CAS  Google Scholar 

  8. J. HIGASHIMURA, O. YAMADA, N. NOHARA, and T. SHIDEI, Intern. J. Appl. Radiation Isotopes, 13 (1962) 308.

    Article  CAS  Google Scholar 

  9. D. L. HORROCKS, Rev. Sci. Instr., 35 (1964) 334.

    Article  CAS  Google Scholar 

  10. F. N. HAYES, Intern. J. Appl. Radiation Isotopes, 1 (1956) 46.

    Article  CAS  Google Scholar 

  11. J. D. DAVIDSON, P. FEIGELSON, Intern. J. Appl. Radiation Isotopes 2 (1957) 13.

    Article  Google Scholar 

  12. A. A. MOGISSI, M. W. CARTER, Anal. Chem., 40 (1968) 812.

    Article  Google Scholar 

  13. J. K. BASSON, J. STEYN, Proc. Phys. Soc., A67 (1954) 297.

    Google Scholar 

  14. J. STEYN, Proc. Phys. Soc., A69 (1955) 865.

    Google Scholar 

  15. D. L. HORROCKS, M. H. STUDIER, Anal. Chem., 36 (1964) 2077.

    Article  CAS  Google Scholar 

  16. G. GOLDSTEIN, Nucleonics, 23 (1965) 67.

    CAS  Google Scholar 

  17. D. L. HORROCKS, M. H. STUDIER, Anal. Chem., 33 (1961) 615.

    Article  CAS  Google Scholar 

  18. M. NOGUCHI, Y. MURAKAMI, 17th Annual Meeting of the Chem. Soc. Japan, Lect. No. 2E07, 1963; Y. MURAKAMI, M. NOGUCHI, S. OHASHI, J. Atomic Energ. Soc. Japan, 7 (1965) 105.

  19. M. NOGUCHI, Radioisotopes, 13 (1964) 362.

    CAS  Google Scholar 

  20. USAEC Rept., NYO-4700.

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Homma, Y., Murakami, Y. Study on the applicability of the integral counting method for the determination of226Ra in various sample forms using a liquid scintillation counter. J. Radioanal. Chem. 36, 173–184 (1977). https://doi.org/10.1007/BF02516265

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02516265

Keywords

Navigation