Abstract
The interaction of 1,3-diaminopropane with glyoxal and NaOCl in water at pH 9.5–10.5 afforded the previously unknown 6,6′-bis(1,5-diazabicyclo[3.1.0]hexane). According to X-ray diffraction data, both bicyclic fragments of the title compound adopt a boat conformation.
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Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 3, pp. 623–625, March, 1999.
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Kuznetsov, V.V., Makhova, N.N. & Dekaprilevich, M.O. 6,6′-Bis(1,5-diazabicyclo[3.1.0]hexane). Russ Chem Bull 48, 617–619 (1999). https://doi.org/10.1007/BF02496194
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DOI: https://doi.org/10.1007/BF02496194