Russian Chemical Bulletin

, Volume 46, Issue 5, pp 1032–1033 | Cite as

Reaction ofN-(3,3,3-trifluoro-2-trifluoromethylprop-1-enyl)dimethylamine with MgSO4·7H2O. Synthesis of 4,4-difluoro-5-trifluoromethyl-2-(2,2,2-trifluoro-1-trifluoromethylethyl)-4H-1,3-dioxine andcis/trans-3-dimethylamino-2-trifluoromethacryloyl fluoride

  • A. V. Popov
  • A. N. Pushin
  • E. L. Luzina
Brief Communications

Abstract

4,4-Difluoro-5-trifluoromethyl-2-(2,2,2-trifluoro-1-trifluoromethylethyl)-4H-1,3-dioxine andcis/trans-3-dimethylamino-2-trifluoromethacryloyl fluoride were obtained by reaction ofN-(3,3,3-trifluoro-2-trifluoromethylprop-1-enyl)dimethylamine with MgSO4·7H2O.

Key words

polyfluroinated enamines, hydrolysis 4,4-difluoro-5-trifluoromethyl-2-(2,2,2-trifluoro-1-trifluoromethylethyl)-4H-1,3-dioxine, formation, decomposition 3-dimethylamino-2-trifluoromethylacryloyl fluoride 3,3,3-trifluoropropanal 

References

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Copyright information

© Plenum Publishing Corporation 1997

Authors and Affiliations

  • A. V. Popov
    • 1
  • A. N. Pushin
    • 1
  • E. L. Luzina
    • 1
  1. 1.Institute of Physiologically Active SubstancesRussian Academy of SciencesChernogolovkaRussian Federation

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