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Sulfur ylides 8.* synthesis of 5-methylthio-7,8-dihydro-4,8a-diazfluorene-6,9-dione

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Abstract

Intramolecular cyclization of ketostabilized sulfur ylide obtained from β-alanine and 2,3-pyridinedicarboxylic anhydride was studied. The structure of the reaction product, 5-methylthio-7,8-dihydro-4,8a-diazafluorene-6,9-dione, was established by X-ray diffraction analysis.

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References

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Authors and Affiliations

  1. Institute of Organic Chemistry, Ufa Research Center for Russian Academy of Sciences, 71 prosp. Oktyabrya, 450054, Ufa, Russian Federation

    F. Z. Galin, S. N. Lakeev, L. F. Chertanova & G. A. Tolstikov

Authors
  1. F. Z. Galin
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  2. S. N. Lakeev
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  3. L. F. Chertanova
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  4. G. A. Tolstikov
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Additional information

For Part 7, see Ref. 1.

Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 11, pp. 2376–2378, November, 1998.

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Galin, F.Z., Lakeev, S.N., Chertanova, L.F. et al. Sulfur ylides 8.* synthesis of 5-methylthio-7,8-dihydro-4,8a-diazfluorene-6,9-dione. Russ Chem Bull 47, 2304–2306 (1998). https://doi.org/10.1007/BF02494303

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  • DOI: https://doi.org/10.1007/BF02494303

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