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Determination of streptomycin in eggs yolk by capillary electrophoresis

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Summary

A capillary electrophoresis method for the determination of streptomycin in eggs is described. Analyses were performed on an uncoated silica capillary using a buffer solution of 30 mM sodium dihydrophosphate, 5 mM boric acid and 5 mM sodium tetraborate. Analytes were detected at 200 nm an the calibration curve was linear over the range of 0.16 to 2.0 μg g−1 (r=0.999). The total analysis time was 7 min. The method has been successfully applied to the quantitative determination of streptomycin in hen eggs after drug ingestion and could used for evaluation of maximum residue limits.

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References

  1. J. F. Prescolt, J. D. Baggot, Antibacterial therapy in veterinary medicine, Iowa State University Press, Ames (1993).

    Google Scholar 

  2. V. Hormazabal, M. Yndestad, J. Liq. Chromatogr.,18, 2695 (1995).

    CAS  Google Scholar 

  3. G. C. Gerhardt, C. D. C. Salisbury, J. D. MacNeil, J. AOAC Int.,77, 765 (1994).

    CAS  Google Scholar 

  4. N. Kurosawa, S. Kuribayashi, E. Owada, K. Ito, M. Nioka, M. Arakawa, R. Fukuda, J. Chromatogr.,343, 379 (1985).

    CAS  Google Scholar 

  5. T. J. Whall, J. Chromatogr.,219, 89 (1981).

    Article  CAS  Google Scholar 

  6. C. L. Flurer, J. Pharm. Biomed Anal.,13, 809 (1995).

    Article  CAS  Google Scholar 

  7. Codex Committee on Residues of Veterinary Drugs in Foods 1997.

  8. Residues of Certain Veterinary Drugs in Foods, A summary of the conclusions of the Joint FAO WHO Expert Committee on Food Additives (JECFA) at its 48th meeting: Geneva. 18–27 February 1997.

  9. Joint FAO/WHO Expert Committee on Food Additives. Fortyseventh Meeting, Rome, 4–13 June 1996.

  10. The European Agency for the Evaluation of Medical Products; Committee for Veterinary Medical Products; Streptomycin and Dihydrostreptomycin-Summary Reports 1995.

  11. S. Horii, J. Liq. Chromatogr.,17, 213 (1994).

    CAS  Google Scholar 

  12. H. Poiger, Ch. Schlatter, Analyst.101, 808 (1976).

    Article  CAS  Google Scholar 

  13. J. P. Sharma, R. F. Bevill, J. Chromatogr.,166, 213 (1978).

    Article  CAS  Google Scholar 

  14. W. J. Blanchflower, R. J. McCracken, A. S. Haggan, D. G. Kennedy, J. Chromatogr. B,692, 351 (1997).

    CAS  Google Scholar 

  15. J. A. Tarbin, G. Shearer, J. Chromatogr.,579, 177 (1992).

    CAS  Google Scholar 

  16. T. Vartiainen, A. Hallikainen, Fresenius J. Anal. Chem.,348, 150 (1994).

    Article  CAS  Google Scholar 

  17. S. E. Katz, C. A. Fassbender, J. J. Dowling, J. AOAC Int.,56, 77 (1973).

    CAS  Google Scholar 

  18. M. Koketsu, L. R. Juneja, M. Kim, M. Ohta, F. Matsuura, T. Yamamoto, J. Food Sci.,58, 743 (1993).

    Article  CAS  Google Scholar 

  19. S. Hoffstetter-Kuhn, A. P. E. Gassmann, H. M. Widmer, Anal. Chem.63, 1541 (1991).

    Article  CAS  Google Scholar 

  20. Dihydrosteptomicin and streptomycin in: Evaluation of certain veterinary drug residues in food. WHO Technical Report Series, Geneva879, 25 (1998).

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Authors and Affiliations

  1. Faculty of Pharmacy, Medical University of Gdansk, Hallera 107, 80416, Gdansk, Poland

    P. Kowalski, I. Oledzka & H. Lamparczyk

  2. Vetos-Pharma, Dzierzoniowska 21, 58260, Bielawa, Poland

    P. Okoniewski

  3. Department of Pharmacology and Toxicology, Agricultural University of Wroclaw, Norwida 31, 50375, Wroclaw, Poland

    M. Switala

Authors
  1. P. Kowalski
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  2. I. Oledzka
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  3. P. Okoniewski
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  4. M. Switala
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  5. H. Lamparczyk
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Kowalski, P., Oledzka, I., Okoniewski, P. et al. Determination of streptomycin in eggs yolk by capillary electrophoresis. Chromatographia 50, 101–104 (1999). https://doi.org/10.1007/BF02493625

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  • DOI: https://doi.org/10.1007/BF02493625

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