Skip to main content
SpringerLink
Log in

Solid-phase microextraction coupled with gas chromatography and gas chromatography—Mass spectrometry for public health pesticides analysis

  • Originals
  • Gas Chromatography
  • Published:
Chromatographia Aims and scope Submit manuscript

Summary

Public health pesticides in two-component mixed solutions were analyzed using solid-phase microextraction (SPME) coupled with gas chromatography (GC) and gas chromatography—mass spectrometry (GC-MS). The two-component mixed solutions used were allethrin mixed with cyfluthrin, cypermethrin mixed with tetramethrin, and transfluthrin mixed with cyfluthrin. Quantitative SPME-GC and SPME-GC-MS analyses using calibration and standard addition methods were evaluated. Using SPME pretreatment saved several tens to hundreds of mL of organic solvent. Quantitative analyses of the SPME-GC and SPME-GC-MS using the calibration and standard addition methods showed promise for simple, fast, and solventless public health pesticide analysis.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. “Household Pesticides”, PJB publication Ltd, Geneva,1994.

  2. “Organophosphorus insecticides: A general introduction”, World Health Organization, Geneva,1986.

  3. “Farm Chemicals Handbook”, Willoughby, Ohio, Meister Publishing Company,1985.

  4. Centner, T.J.Occup. Health and Ind. Med. 1998,39, 205.

    Google Scholar 

  5. Centner, T.J.; Gunter, L.F.Environ. Int. 1999,25, 635–646.

    Article  Google Scholar 

  6. Fassen, R.Eur. Water Pollut. Control 1995,5, 34–40.

    Google Scholar 

  7. Lewalter, J.; Leng, G.Toxicol. Lett. 1999,107, 131–144.

    Article  CAS  Google Scholar 

  8. Arbuckle, T.E.; Sever, L.E.Occup. Health and Ind. Med. 1998,39, 151.

    Google Scholar 

  9. Bowles, R.G.; Webster, J.P.G.Crop Protect. 1995,14, 593–600.

    Article  Google Scholar 

  10. Richardson, M.Wat. Sci. Tech. 1999,37(8), 19–25.

    Article  Google Scholar 

  11. “Advances in Pesticide Formulation Technology”, American Chemical Society, Washington D.C.,1984.

  12. Zhang, Z.; Yang, M.; Pawliszyn, J.Anal. Chem. 1994,66, 844A-853A.

    CAS  Google Scholar 

  13. Buchholz, K.; Pawliszyn, J.Anal. Chem. 1994,66, 160–167.

    Article  CAS  Google Scholar 

  14. Pawliszyn, J. “Solid phase microextraction-theory and practice”, New York, Wiley-VCH,1997.

    Google Scholar 

  15. Lee, M.R.; Lee, R.I.; Lin, Y.W.; Chen, C.M.; Hwang, B.H.Anal. Chem. 1998,70, 1963–1968.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Applied Chemistry, National Chi Nan University, 1, University Road, 545, Puli, Nantou, Taiwan

    C. BorFuh

  2. Department of Applied Chemistry, Chaoyang University of Technology, 168 Gifeng East Road, 413, Wufeng, Taichung County, Taiwan

    Y. C. Yang & L. S. Ho

  3. School of Applied Chemistry, Chung Shan Medical University, 110, Sec 1, Chien-kuo N. Road, 402, Taichung, Taiwan

    H. Y. Tsai

Authors
  1. C. BorFuh
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Y. C. Yang
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. H. Y. Tsai
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. L. S. Ho
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

BorFuh, C., Yang, Y.C., Tsai, H.Y. et al. Solid-phase microextraction coupled with gas chromatography and gas chromatography—Mass spectrometry for public health pesticides analysis. Chromatographia 57, 525–528 (2003). https://doi.org/10.1007/BF02492552

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02492552

Key Words

Search

Navigation