Summary
Gas chromatography-mass spectrometry with headspace solid-phase microextraction was used for the analysis of the volatile constituents of celery and water dropwort. Solid-phase microextraction was carried out with a 65 μm polydimethylsiloxane-divinylbenzene fiber at 60°C for 45 min. The fiber was desorbed in the GC injection liner at 250°C for 3 min. Thirty-eight compounds in celery and thirty-five compounds in water dropwort were separated and identified. The main compounds found in both celery and water dropwort includedcis-3-hexen-1-ol, α-myrcene, limonene, a-pinene, 1,4-cyclohexadiene, 1,5,5-trimethyl-6-methylene-cyclohexene, 3,7,11,15-tetramethyl-2-hexadecen-1-ol,n-hexadecanoic acid and α-caryophyllene. The precision of the method was studied by five replicate analysis of the main valatile compounds in celery and a relative standard deviation value less than 5.0% showed that the method could provide good reproducibility.
Similar content being viewed by others
References
Nuo, X.L.; Gao, W.Z.Flora Popularis Sinicae Chinese Science Press 1999.
Zhao, Y.S.Chinese Condiment 2000,8, 15–19.
Xia, W.; Sui, H.P.China Public Health 2001,17, 337–341.
Philippe, J.; Suvarnalatha, G.; Sankar, R.; Suresh, S.J. Essent. Oil. Res. 2002,14, 276–277.
Rao, L.J.M.; Nagalakshmi, S.; Naik J.P.; Shankaracharya, N.B.J. Food Sci. Tech. Mys. 2000,37, 631–635.
Zhang, X.M.China Public health 2001,17, 332–336.
Arthur, C.; Pawliszyn, J.Anal. Chem. 1990,62, 2145–2154.
Mariaca, R.; Bosset, J.O.Lait 1997,77, 13–18.
Sedlakova, J.; Matisova, E.; Slezackova, M.Chem. Listy 1998,92, 633–639.
Kataoka, H.; Lord, H.L.; Pawliszyn, J.J. Chromatogr. A 2000,880, 35–43.
Ulrich, S.J. Chromatogr. A 2000,902, 167–175.
Deng, C.H.; Song, G.X.; Hu, Y.M.; Zhang, X.M.Chromatographia (under publication).
Shang, C.Q.; Hu, Y.M.; Deng, C.H.; Hu, K.J.J. Chromatogr. A 2002,942, 283–288.
Shang, C.Q.; Deng, C.H.; Zhang, X.Y.; Chen, Z.F.; Hu, Y.M.Chromatographia.2002,55, 737–741.
Zhang, Z.; Yang, M.Anal. Chem. 1994,66, 844–853.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Deng, C., Song, G., Zheng, X. et al. Analysis of the volatile constituents ofApium graveolens L. andOenanthe L. by gas chromatography-mass spectrometry, using headspace solid-phase microextraction. Chromatographia 57, 805–809 (2003). https://doi.org/10.1007/BF02491769
Received:
Revised:
Accepted:
Issue Date:
DOI: https://doi.org/10.1007/BF02491769