Chromatographia

, Volume 53, Issue 5–6, pp 306–310 | Cite as

Determination of triazines and amides in water using solid phase microextraction coupled with GC-MS

  • R. Hu
  • D. Elia
  • J. -M. Berthion
  • S. Poliak
Originals Gas Chromatography

Summary

Solid phase microextraction was coupled with gas chromatography-mass spectrometry (SPME-GC-MS) to screen for sixteen nitrogen-containing compounds, including herbicides, in water samples. The effects of stirring, extraction time, pH, salt concentration and the choice of fiber coating material were evaluated. The repeatability was in the range of 0.72–18.2 (CV % at 200 ng·L−1) and the reproducibility, in the range of 5.4–34 (at 500 ng·L−1).

Key Words

Gas chromatography-mass spectrometry Solid phase microextraction Triazines Amides Water pollution 

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Copyright information

© Friedr. Vieweg & Sohn Verlagsgesellschaft mbH 2001

Authors and Affiliations

  • R. Hu
    • 1
  • D. Elia
    • 2
  • J. -M. Berthion
    • 1
  • S. Poliak
    • 1
  1. 1.Laboratoire Départemental de la SartheLe Mans CedexFrance
  2. 2.Dipartimento di TossicologiaUniversità di CagliariCagliariItaly

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