Fresenius' Zeitschrift für analytische Chemie

, Volume 328, Issue 4–5, pp 324–329 | Cite as

Analysis of solid samples by graphite furnace atomic emission spectrometry

  • D. C. Baxter
  • W. Frech
Lectures Theory and Instrumentation

Summary

The possibility of determining a range of analytes in solid samples using a single set of optimised ‘multi-element’ instrumental parameters for a graphite furnace atomic emission spectrometry (GFAES) system was investigated. Accurate results for silver, manganese, nickel, lead and vanadium in solid reference materials of biological origin were obtained using peak area evaluation and calibration against standard solution curves. The versatility of the constant-temperature atomiser enabled lead and silver in metallurgical samples to be determined as well, although quantification against standard steel materials was necessary in the case of silver to obtain acceptable results.

Keywords

Nickel Graphite Manganese Vanadium Reference Material 

Analyse von Feststoffproben durch Graphitofen-AES

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. 1.
    Marshall J, Littlejohn D, Ottaway JM, Harnly JM, Miller-Ihli NJ, O'Haver TC (1983) Analyst 108:178CrossRefGoogle Scholar
  2. 2.
    Falk H, Hoffman E, Lüdke Ch (1984) Spectrochim Acta 39B:283CrossRefGoogle Scholar
  3. 3.
    Grobenski Z, Lehmann R, Welz B (1981) Paper 260 presented at 32nd Pittsburgh Conf Anal Chem Appl Spectrosc, Atlantic City, NJ, USAGoogle Scholar
  4. 4.
    Marshall J, Giri SK, Littlejohn D, Ottaway JM (1983) Anal Chim Acta 147:173CrossRefGoogle Scholar
  5. 5.
    Frech W, Baxter DC, Hütsch B (1986) Anal Chem 58:1973CrossRefGoogle Scholar
  6. 6.
    Littlejohn D, Ottaway JM (1977) Analyst 102:553CrossRefGoogle Scholar
  7. 7.
    Lundberg E, Baxter DC, Frech W (1986) J Anal At Spectrom 1:105CrossRefGoogle Scholar
  8. 8.
    Bezur L, Marshall J, Ottaway JM, Fakhrul-Aldeen R (1983) Analyst 108:553CrossRefGoogle Scholar
  9. 9.
    Falk H, Hoffmann E, Lüdke Ch, Schmidt KP (1986) Spectrochim Acta 41B:853CrossRefGoogle Scholar
  10. 10.
    Marshall J, Littlejohn D, Ottaway JM, Miller-Ihli NJ, O'Haver TC, Harnly JM (1984) Spectrochim Acta 39B:321CrossRefGoogle Scholar
  11. 11.
    Grobenski Z, Lehmann R, Tamm R, Welz B (1982) Mikrochim Acta 1:115CrossRefGoogle Scholar
  12. 12.
    Harnly JM, Miller-Ihli NJ, O'Haver TC (1984) Spectrochim Acta 39B:305CrossRefGoogle Scholar
  13. 13.
    Epstein MS, Rains TC, O'Haver TC (1976) Appl Spectrosc 30:324CrossRefGoogle Scholar
  14. 14.
    Langmyhr FJ, Wibetoe G (1985) Prog Anal At Spectrosc 8:193Google Scholar
  15. 15.
    Lundberg E, Frech W (1979) Anal Chim Acta104:75CrossRefGoogle Scholar
  16. 16.
    Lundberg E, Frech W (1979) Anal Chim Acta 108:75CrossRefGoogle Scholar
  17. 17.
    Bäckman SE, Karlsson RW (1979) Analyst 104:1017CrossRefGoogle Scholar

Copyright information

© Springer-Verlag 1987

Authors and Affiliations

  • D. C. Baxter
    • 1
  • W. Frech
    • 1
  1. 1.Department of Analytical ChemistryUniversity of UmeåUmeåSweden

Personalised recommendations