Abstract
A rapid and reliable method for determination of90Sr in soil and sediment has been developed. The method is based on lithium-borate fusion and extraction chromatography with a Sr-resin. The samples can be dissolved and separated for Sr in approximately 5 hours of which the fusion and dissolution requires 20 minutes. The method has been applied to four reference materials, two soils and two sediments, and the results agree well with the recommended values. The mean recovery of Sr was 71%.
Similar content being viewed by others
References
D. H. Oughton, B. Salbu, T. L. Brand, J. P. Day, A. Aarkrog, Analyst, 118 (1993) 1101.
I. Friberg, J. Radioanal. Nucl. Chem., 226 (1997) 55.
C. O. Ingamells, Anal. Chim. Acta, 52 (1970) 323.
R. Bock, A Handbook in Decomposition Methods in Analytical Chemistry, The Blackie Group, London, 1979, p. 93.
C. W. Sill, K. W. Puphal, F. D. Hindman, Anal. Chem., 46 (1974) 1725.
H. Bennet, G. J. Oliver, Analyst, 101 (1976) 803.
J. Eastell, J. P. Willis, X-ray Spectrom., 19 (1990) 3.
F. Claisse, Glass Disks and Solutions by Fusion in Borates for Users of Claisse Fluxers, Corporation Scientifique Claisse Inc., Sainte-Foy, Quebec, Canada, 1995.
N. Vajda, A. Gohds-Esphahani, E. Cooper, P. R. Danesi, J. Radioanal. Nucl. Chem., 162 (1992) 307.
I. Croudace, P. Warwick, R. Taylor, S. Dee, Anal. Chim. Acta, 371 (1998) 217
E. P. Horwitz, R. Chiarizia, M. L. Dietz, Solv. Extr. Ion Exch., 10 (1992) 313.
C. Pin, D. Briot, C. Bassin, F. Poitrasson, Anal. Chim. Acta, 298 (1994) 209.
S. Ballestra, J. Gastaud, J. J. Lopez, P. Parisi, D. Vas, Intercomparison of Radionuclide Measurements in Marine Sediment Sample IAEA-135, IAEA/AL/063, IAEA Marine Environmental Laboratory, B.P. No. 800, MC 98012 Monaco Cedex, 1993.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Nygren, U. Determination of90Sr in soil and sediment using lithium-borate fusion and extraction chromatography. J Radioanal Nucl Chem 241, 549–551 (1999). https://doi.org/10.1007/BF02347211
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF02347211