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A normal-incidence reflective polariscope for viscoelasticity measurements

An instrument capable of measuring isoclinics and isochromatics as a function of time was used to determine strains in solid propellant

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Abstract

A normal-incidence reflective polariscope, together with some auxiliary instrumentation, is described. The instrument consists of eight unit polariscopes, relatively oriented, which are indexed into position within a short period of time to obtain a set of eight data. These data provide sufficient information to separate the principal strains obtained at different time intervals. The primary experimental objective was to design an inflated-cylinder test, analogous to the loading experienced in a solid-propellant rocket, that would enable reasonable measurements of the triaxial surfacelayer strains of a viscoelastic material as a function of time. The stress geometry imposed on the viscoelastic material was that of an unrestricted, biaxially pressurized, thick-walled tubular cylinder. The material investigated was polyurethane solid propellant. Two different methods to reduce the biaxial strains in a low-modulus birefringent polyurethane coating are also described.

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Abbreviations

C :

stress-optic constant, psi−1

E :

Young's modulus, psi

e 33 :

thickness strain of the coating

n :

number of points being investigated

n 11 :

refractive index in the 11 privileged direction

n 22 :

refractive index in the 22 privileged direction

t :

coating thickness at any state of strain, in

t 0 :

original coating thickness, in

x i :

distance from a pointi on the reference radial trace to the shear plane ψ, in

y n :

distance from symmetrical center of cylinder to point under investigation, in

x,y,z :

Cartesian coordinate system (z thickness of coating)

δ:

equal increment on the radial trace=(y 1 −y n )/(n−1)

11 :

principal strain in the 11 privileged direction

22 :

principal strain in the 22 privileged direction

33 :

longitudinal strain of the thick-walled cylinder

θ:

reference angle, deg

μ:

Poisson's ratio

σ 11 :

principal stress in the 11 privileged direction

σ 22 :

principal stress in the 22 privileged direction

σ ψ :

shear stress, psi

ψ:

angle at which shear acts, deg

References

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This paper presents the results of one phase of research carried out at the Jet Propulsion Laboratory, California Institute of Technology, under ARPA Contract Letter Order No. 107-60 and NAS 7-100 sponsored by the National Aeronautics and Space Administration.

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San Miguel, A., Silver, R.H. A normal-incidence reflective polariscope for viscoelasticity measurements. Experimental Mechanics 5, 345–352 (1965). https://doi.org/10.1007/BF02327538

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