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A sandwich tank for continuous quasi-column development of precoated high-performance thin-layer chromatography plates

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Summary

A simple home-made sandwich tank of Brenner-Niederwieser type is described in which the solvent is delivered to the thin-layer from a small container by a capillary siphon using a device which distributes the solvent at right angles to the direction of development. The samples can be spotted behind the line of solvent demixing which in some cases greatly improves the quality of chromatograms (reduced tailing). The development requires only 10% of the amount of solvent normally used in saturated tanks.

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References

  1. E. Soczewiński, J. Chromatogr.138, 443 (1977).

    Google Scholar 

  2. E. Soczewiński, Chem. Anal. (Warsaw)23, 515 (1978).

    Google Scholar 

  3. E. Soczewiński, Pol. Pat. P-197 729.

  4. M. Brenner andA. Niederwieser, Experientia (Basel)17, 237 (1961).

    CAS  Google Scholar 

  5. A. Zlatkis andR. E. Kaiser (Eds.), HPTLC — High Performance Thin-Layer Chromatography, Elsevier, Amsterdam 1977.

    Google Scholar 

  6. E. Soczewiński andJ. Kuczmierczyk, J. Chromatogr.150, 53 (1978).

    Google Scholar 

  7. L. R. Snyder, Anal. Chem.46, 1384 (1974).

    Article  CAS  Google Scholar 

  8. H. G. Cassidy, Fundamentals of Chromatography, in Technique of Organic Chemistry (A. Weissberger, Ed.), Vol. 10, Wiley (Interscience) New York 1957, p. 198f.

    Google Scholar 

  9. E. Soczewiński andH. Szumito, to be published.

  10. S. Hara, J. Chromatogr.137, 41 (1977).

    Article  CAS  Google Scholar 

  11. A. M. Siouffi, A. Guillemonat andG. Guiochon, J. Chromatogr.137, 35 (1977).

    Article  CAS  Google Scholar 

  12. F. Geiss, Die Parameter der Dünnschicht-Chromatographie, Vieweg Braunschweig 1973, p. 176f.

    Google Scholar 

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Soczewiński, E., Wawrzynowicz, T. A sandwich tank for continuous quasi-column development of precoated high-performance thin-layer chromatography plates. Chromatographia 11, 466–468 (1978). https://doi.org/10.1007/BF02314787

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  • DOI: https://doi.org/10.1007/BF02314787

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