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Attempts on the semi-preparative resolution of racemic esters of aminoacids on a chiral liquid chromatographic column derived from N-formylisoleucine

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Summary

A semi-preparative (250mm×10mm i.d.) chiral liquid chromatographic column incorporating a chiral material derived from N-formylisoleucine has been found to be suitable for the resolution of milligram or larger quantities of two aminoacid esters. The method should be capable of being used for other racemic materals on an even larger scale.

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References

  1. J. N. Akanya, D. R. Taylor, J. Liq. Chromatogr.,10, (5), 805 (1987).

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  2. J. N. Akanya, S. M. Hitchen, D. R. Taylor, Chromatographia,16, 224 (1982).

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Authors and Affiliations

  1. Department of Chemistry, School of Science and Science Education, Federal University of Technology, P. O. Box 656, Minna, Nigeria

    J. N. Akaya

  2. Chemistry Department, University of Manchester, Institute of Science and Technology, M60, 1QD, Manchester, UK

    D. R. Taylor

Authors
  1. J. N. Akaya
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  2. D. R. Taylor
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Akaya, J.N., Taylor, D.R. Attempts on the semi-preparative resolution of racemic esters of aminoacids on a chiral liquid chromatographic column derived from N-formylisoleucine. Chromatographia 25, 923–924 (1988). https://doi.org/10.1007/BF02311432

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  • DOI: https://doi.org/10.1007/BF02311432

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