Skip to main content
Log in

Analysis of some organochlorine pesticides in seafood samples by solid-phase extraction—Gas chromatography

  • Originals
  • Published:
Chromatographia Aims and scope Submit manuscript

Summary

The use of the solid-phase extraction technique for the rapid sample preparation of organochlorine pesticides is described. Samples were simultaneously extracted, cleaned, and fractionated by the solid-phase extraction method and a further separation and determination of extracted fractions was carried out by gas chromatography with either an electron capture or a Hall electrolytic conductivity detector. The percent recovery of the extracted seven pesticides was compared to that of the conventional liquid-liquid extraction method. The analytical figures of merit., chromatograms, and statistic data are reported. The application of this method was demonstrated by a real fish sample determination with mass spectra for confirmation of Kepone detection.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. H. Freiser, “Solvent Extraction”, in An Introduction to Separation Science,B. L. Karger, L. R. Snyder, C. Horvath, eds., John Wiley & Sons, New York, 1973, pp. 247–263.

    Google Scholar 

  2. “Baker-10 SPE Applications Guide”, Vols. I & II, J. T. Baker Chemical Co., Phillipsburg, NJ (1982 & 1984).

  3. “1985 Buyers' Guide & Merchandising Directory”, LC Magazine,3, (8), 722 (1985).

  4. B. A. Bidlingmeyer, LC Magazine,2, (8), 578 (1984).

    CAS  Google Scholar 

  5. “Pesticide Analytical Manual Vol. 1: Methods Which Detect Multiple Pesticides”, Method 211.14, U.S. Department of Health & Human Sciences, Food and Drug Administration, Washington, DC.

  6. “Compliance Program Evaluation FY-77-Kepone and Mirex Contamination”, U.S. Environmental Protection Agency, Health Effects Research Laboratory, Research Triangle Park, NC, Dec.16, 1975.

  7. J. N. Huckins, D. L. Stalling, J. D. Petty, D. R. Buckler, B. T. Johnson, J. Agr. Food Chem.,30, 1020 (1982).

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Kohler, P.W., Su, S.Y. Analysis of some organochlorine pesticides in seafood samples by solid-phase extraction—Gas chromatography. Chromatographia 21, 531–537 (1986). https://doi.org/10.1007/BF02310541

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02310541

Key Words

Navigation