Chromatographia

, Volume 13, Issue 10, pp 651–660 | Cite as

Preparation of glass capillary columns

  • G. Alexander
Green pages

Summary

Glass capillary column chromatography is the most rapidly growing part of gas chromatography. There are many complex new analytical tasks and they require special capillary columns. Fortunately there is a wide range of column preparation methods available, and they make the preparation of glass capillary columns a more varied job than that of packed columns. In this paper these methods are reviewed and suggestions are given for making task-oriented columns.

Key Words

Capillary columns, glass Gas chromatography Column preparation 

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References

  1. [1]
    Industrial Research and Development21, (2) 96 Feb., 1979.Google Scholar
  2. [2]
    Journal of High Resolution Chromatography and Chromatography Communications.Google Scholar
  3. [3]
    W. Jennings, Gas Chromatography With Glass Capillary Columns. Acad. Press, New York, 1978.Google Scholar
  4. [4]
    K. Grob, Chromatographia8, 423 (1975).CrossRefGoogle Scholar
  5. [5]
    G. Schomburg andH. Hussmann, Chromatographia8, 517 (1975).CrossRefGoogle Scholar
  6. [6]
    J. Roerade Chromatographia8, 511 (1975).Google Scholar
  7. [7]
    G. Schomburg, H. Hussmann andF. Weeke, Chromatographia10, 580 (1977).CrossRefGoogle Scholar
  8. [8]
    P. Sandra andM. Verzele, Chromatographia10, 419 (1977).CrossRefGoogle Scholar
  9. [9]
    F. I. Onuska andM. E. Comba, Chromatographia10, 498 (1977).CrossRefGoogle Scholar
  10. [10]
    D. H. Parker andJ. L. Marshall inR. E. Kaiser Ed., Proc. 2nd Intern. Symp. on Glass Capillary Chromatography, Hindelang, Germany, 1977, Inst. of Chrom. Bad Dürkheim, 1977, p. 299.Google Scholar
  11. [11]
    A. Liberti andG. C. Goretti, ibid. Proc. 2nd Intern. Symp. on Glass Capillary Chromatography, Hindelang, Germany, 1977. Inst. of Chrom. Bad Dürkheim, 1977, p. 231.Google Scholar
  12. [12]
    G. Schomburg, J. High. Res. Chrom. and Chrom. Comm.2, 461 (1979).Google Scholar
  13. [13]
    M. Verzele andP. Sandra, ibid,2, 303 (1979).Google Scholar
  14. [14]
    M. Novotny, Anal. Chem.50, 16A (1978).Google Scholar
  15. [15]
    K. Grob andG. Grob, J. High. Res. Chrom. and Chrom. Comm.2, 109 (1979).Google Scholar
  16. [16]
    M. Novotny andA. Zlatkis, Chromatogr. Rev.14, 1 (1971).Google Scholar
  17. [17]
    L. S. Ettre, Open Tubular Columns in Gas Chromatography, Plenum Press, New York, 1965, p. 19.Google Scholar
  18. [18]
    W. Bertsch, F. Shunbo, R. C. Chang andA. Zlatkis, Chromatographia7, 128 (1974).CrossRefGoogle Scholar
  19. [19]
    W. Espe, Werkstoffkunde der Hochvakuumtechnik, VEB Deutscher Verlag der Wiss., Berlin 1960, p. 9, 13.Google Scholar
  20. [20]
    H. Borwitzky andG. Schomburg, J. Chromatogr.170, 99 (1979).CrossRefGoogle Scholar
  21. [21]
    A. M. Filbert inI. I. Domsky andJ. A. Perry Eds. Recent Advances in Gas Chromatography, M. Dekker, New York 1971, p. 49.Google Scholar
  22. [22]
    R. D. Dandeneau andE. H. Zerenner, J. High Res. Chrom. and Chrom. Comm.2, 351 (1979).Google Scholar
  23. [23]
    D. H. Desty, J. H. Haresnape andB. H. F. Whyman, Anal. Chem.32, 302 (1960).CrossRefGoogle Scholar
  24. [24]
    E. A. Mistryukov, L. S. Savichev andV. V. Gavrilov in Proc. 2nd “Danube” Symp., Karlsbad, Chechoslovakia, 1979. Chechosl. Chem. Soc., 1979. B. 2.21.Google Scholar
  25. [25]
    D. H. Desty andA. A. Douglas, J. Chromatogr.142, 39 1977.Google Scholar
  26. [26]
    D. H. Desty andA. A. Douglas, J. Chromatogr.158, 73 (1978).Google Scholar
  27. [27]
    A. M. Filbert andM. L. Hair, J. Gas Chromatogr.6, 150 (1968).Google Scholar
  28. [28]
    A. M. Filbert andM. L. Hair, J. Gas. Chromatogr.6, 219 (1968).Google Scholar
  29. [29]
    K. Grob andG. Grob, J. Chromatogr.125, 471 (1976).CrossRefGoogle Scholar
  30. [30]
    G. Alexander andH. Zimmer, Lecture presented at 13th Intern. Symp. on Advances of Chromatogr. Oct. 16–18, 1978. St. Louis, Mo. USA.Google Scholar
  31. [31]
    M. L. Lee, D. L. Vassilaros, L. V. Phillips, M. D. Hercules, H. Azumaya, J. W. Jorgenson, M. P. Maskarinec andM. Novotny, Anal. Letters12 A2, 191 (1979).Google Scholar
  32. [32]
    F. I. Onuska, B. K. Afghan andR. J. Wilkinson, J. Chromatogr.158, 83 (1978).Google Scholar
  33. [33]
    W. G. Jennings, K. Yabumoto andR. H. Wohleb, J. Chromatogr. Sci.12, 344 (1974).Google Scholar
  34. [34]
    J. Simon andL. Szepesy, J. Chromatogr.119, 495 (1976).CrossRefGoogle Scholar
  35. [35]
    G. Alexander andG. A. F. M. Rutten, J. Chromatogr.99, 81 (1974).Google Scholar
  36. [36]
    G. A. F. M. Rutten andJ. A. Luyten, J. Chromatogr.74, 177 (1972).CrossRefGoogle Scholar
  37. [37]
    G. Alexander, G. Garzó andG. Pályi, J. Chromatogr.91, 25 (1974).Google Scholar
  38. [38]
    M. Novotny andK. Grohman, J. Chromatogr.84, 167 (1973).Google Scholar
  39. [39]
    R. N. Wenzel, Ind. Eng. Chem.28, 988 (1936).CrossRefGoogle Scholar
  40. [40]
    K. Tesarik andM. Novotny inH. G. Struppe Ed., Gaschromatographie 1968. Akademie-Verlag, Berlin, 1968, p. 755.Google Scholar
  41. [41]
    G. Alexander andG. A. F. M. Rutten, Chromatographia6, 231 (1973).Google Scholar
  42. [42]
    J. J. Franken, G. A. F. M. Rutten andJ. A. Rijks, J. Chromatogr.126, 117 (1976).Google Scholar
  43. [43]
    J. Krupcik, M. Kristin, M. Valichovicova andS. Janiga, J. Chromatogr.126, 147 (1976).Google Scholar
  44. [44]
    H. T. Badings, J. J. v. d. Pol andD. G. Schmidt, Chromatographia10, 404 (1977).CrossRefGoogle Scholar
  45. [45]
    J. D. Schieke, N. R. Comins andV. Pretorius, J. Chromatogr.112, 97 (1975).CrossRefGoogle Scholar
  46. [46]
    J. D. Schieke, N. R. Comins andV. Pretorius, J. Chromatogr.115, 373 (1975).CrossRefGoogle Scholar
  47. [47]
    F. I. Onuska andM. E. Comba, J. Chromatogr.126, 133 (1976).Google Scholar
  48. [48]
    R. A. Heckman, Ch. R. Green andF. W. Best, Anal. Chem.50, 2157 (1978).Google Scholar
  49. [49]
    A. L. German andE. C. Horning, J. Chromatogr. Sci.11, 76 (1973).Google Scholar
  50. [50]
    A. L. German, C. D. Pfaffenberger, J. P. Thenot, M. G. Horning andE. C. Horning, Anal. Chem.45, 931 (1973).CrossRefGoogle Scholar
  51. [51]
    M. Blumer, Anal. Chem.45, 980 (1973).CrossRefGoogle Scholar
  52. [52]
    E. Schulte andL. Acker, Z. Anal. Chem.268, 260 (1974).CrossRefGoogle Scholar
  53. [53]
    E. Schulte, Chromatographia9, 315 (1976).CrossRefGoogle Scholar
  54. [54]
    C. A. Cramers, E. A. Vermeer andJ. J. Franken, Chromatographia10, 412 (1977).CrossRefGoogle Scholar
  55. [55]
    K. Grob, Chromatographia10, 625 (1977).Google Scholar
  56. [56]
    R. de Nijs, G. A. F. M. Rutten, J. J. Franken, R. P. M. Dooper, andJ. A. Rijks, J. High Res. Chrom. and Chrom. Comm.2, 447 (1979).Google Scholar
  57. [57]
    K. Grob andG. Grob, J. Chromatogr.125, 471 (1976).CrossRefGoogle Scholar
  58. [58]
    K. Grob, J. R. Guenther, andA. Portmann, J. Chromatogr.147, 111 (1978).CrossRefGoogle Scholar
  59. [59]
    K. Grob Jr., G. Grob, andK. Grob, J. High Res. Chrom. and Chrom. Comm.1, 149 (1978).Google Scholar
  60. [60]
    K. Grob, G. Grob, andK. Grob, Jr., J. High Res. Chrom. and Chrom. Comm.2, 31 (1979).Google Scholar
  61. [61]
    J. L. Marshall andM. W. Sanderson, Chromatographia12, 782 (1979).CrossRefGoogle Scholar
  62. [62]
    M. Novotny, J. Chromatogr. Sci.8, 390 (1970).Google Scholar
  63. [63]
    M. Novotny andK. D. Bartle, Chromatographia7, 122 (1973).Google Scholar
  64. [64]
    M. Novotny andK. D. Bartle, Chromatographia3, 272 (1970).Google Scholar
  65. [65]
    Th. Welsch, W. Engewald andCh. Klaucke, Chromatographia10, 22 (1977).Google Scholar
  66. [66]
    K. Grob, personal communication, April 1979.Google Scholar
  67. [67]
    E. J. Malec, J. Chromatogr. Sci.9, 318 (1971).Google Scholar
  68. [68]
    R. E. Kaiser andR. Rieder, Chromatographia9, 491 (1975).Google Scholar
  69. [69]
    C. R. Hastings andW. A. Aue, J. Chromatogr.89, 369 (1974).CrossRefGoogle Scholar
  70. [70]
    D. A. Cronin, J. Chromatogr.97, 263 (1974).CrossRefGoogle Scholar
  71. [71]
    G. Schomburg, H. Hussmann andF. Weeke, J. Chromatogr.99, 63 (1974).Google Scholar
  72. [72]
    J. J. Franken, R. C. M. de Nijs andF. L. Schulting, J. Chromatogr.144, 253 (1977).CrossRefGoogle Scholar
  73. [73]
    R. C. M. De Nijs, J. J. Franken, R. P. M. Dooper, J. A. Rijks, H. J. J. M. de Ruwe andF. L. Schulting, J. Chromatogr.167, 231 (1978).Google Scholar
  74. [74]
    G. Schomburg, H. Hussmann andH. Borwitzky, Chromatographia12, 651 (1979).CrossRefGoogle Scholar
  75. [75]
    A. Venema, L. G. J. v. d. Ven andH. v. d. Seege, J. High Res. Chrom. and Chrom. Comm.2, 69 (1979).Google Scholar
  76. [76]
    G. Dijkstra andJ. de Goey, inD. H.Desty Ed., Gas Chromatography 1958., Butterworths, London, 1958, p. 58.Google Scholar
  77. [77]
    K. D. Bartle, Anal. Chem.45, 1831 (1973).CrossRefGoogle Scholar
  78. [78]
    G. Alexander andS. R. Lipsky, Chromatographia10, 487 (1977).CrossRefGoogle Scholar
  79. [79]
    A. Venema andG. C. v. d. Ven, inR. E. Kaiser Ed., Proc. 2nd Intern. Symp. on Glass Capillary Chromatogr., Hindelang, Germany, 1979. Inst. of Chromatogr., Bad Dürkheim, 1977.Google Scholar
  80. [80]
    J. Bouche andM. Verzele, J. Gas Chromatogr.6, 501 (1968).Google Scholar
  81. [81]
    K. Grob J. High Res. Chrom. and Chrom. Comm.1, 93 (1978).Google Scholar
  82. [82]
    E. L. Ilkova andE. A. Mistryukov, J. Chromatogr. Sci.9, 569 (1971).Google Scholar
  83. [83]
    C. Madani, E. M. Chambaz, M. Rigaud, J. Durand andP. Chebroux, J. Chromatogr.126, 161 (1976).Google Scholar
  84. [84]
    C. Madani, E. M. Chambaz, M. Rigaud, P. Chebroux andJ. C. Breton, Chromatographia10, 466 (1977).CrossRefGoogle Scholar
  85. [85]
    C. Madani andE. M. Chambaz, Chromatographia11, 725 (1978).CrossRefGoogle Scholar
  86. [86]
    L. Blomberg, J. Buijten, J. Gawdzik andT. Wännman Chromatographia11, 521 (1978).Google Scholar
  87. [87]
    L. Blomberg andT. Wännman, J. Chromatogr.168, 81 (1979).CrossRefGoogle Scholar

Copyright information

© Friedr. Vieweg & Sohn Verlagsgesellschaft mbH 1980

Authors and Affiliations

  • G. Alexander
    • 1
  1. 1.Laboratory for Inorganic ChemistryHungarian Academy of SciencesBudapestHungary

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