Summary
Thin-layer and column high-performance liquid chromatography based on amino propyl-modified silica gel using aqueous and non-aqueous mobile phases containing organic modifier and cationic or anionic ion-pairing reagents were used for the determination ofR F andk values of some sulfonamides. The influence of the different organic modifiers and ion-pairing reagents on retention has been compared.
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L. Van Poucke, D. Rousseau, C. Van Peteghem, B. M. J. De Spiegeleer, J. Planar Chromatogr.2, 395 (1989).
L. Lepri, P. G. Desideri, V. Coas, J. Chromatogr.405, 394 (1987).
M. L. Bieganowska, A. Doraczyñska-Szopa, A. Petruczynik, J. Planar Chromatogr.6, 121 (1993).
M. L. Bieganowska, A. Doraczyñska-Szopa, A. Petruczynik, J. Planar Chromatogr.8, 122 (1995).
J. Wieling, J. Schepers, J. Hempenius, C. K. Mensiuk, J. H. G. Jonkman, J. Chromatogr.545, 101 (1991).
L. Lepri, P. G. Desideri, O. Heimler, J. Chromatogr.169, 271 (1979).
J. P. Sharma, E. G. Perkins, R. F. Bevill, J. Pharm. Sci.65, 1606 (1976).
M. L. Bieganowska, Chem. Anal.40, 687 (1995).
M. L. Bieganowska, A. Petruczynik, Chem. Anal.40, 869 (1995).
M. C. Pietrogrande, F. Fondi, P. A. Borea, C. Bighi, J. Chromatogr.471, 407 (1989).
T. Cserati, H. E. Hauck, J. Chromatogr.514, 45 (1990).
R. P. Vinas, C. L. Erroz, A. H. Canals, M. H. Cordoba, Chromatographia40, 382 (1995).
L. V. Walker, J. R. Walsh, J. J. Webber, J. Chromatogr.595, 179 (1992).
A. R. Long, C. R. Short, S. A. Barker, J. Chromatogr.502, 87 (1990).
N. Takeda, Y. Akiyama, J. Chromatogr.607, 31 (1992).
J. Sherma, M. Duncan, J. Liq. Chromatogr.9(9), 1861 (1986).
M. L. Bieganowska, A. Petruczynik, A. Doraczyñska-Szopa, J. Pharm. Biomed. Analysis11, 241 (1993).
M. L. Bieganowska, Chem. Anal.40, 859 (1995).
W. Jost, H. E. Hauck, J. Chromatogr.261, 235 (1983).
E. Soczewiñski, Anal. Chem.41, 179 (1969).
L. R. Snyden, Anal. Chem.46, 1384 (1974).
R. J. Hurtubise, A. Hussain, H. F. Silver, Anal. Chem.53, 1993 (1981).
G. Grassini-Strazza, L. Nicoletti, J. Chromatogr.322, 149 (1985).
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Bieganowska, M.L., Petruczynik, A. Thin-layer and column chromatography of sulfonamides on aminopropyl silica gel. Chromatographia 43, 654–658 (1996). https://doi.org/10.1007/BF02292983
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DOI: https://doi.org/10.1007/BF02292983