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Hydrogenation of 4-(2-furyl)-2-oxobutenoic acid sodium salt on Raney nickel

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

The hydrogenation of 4-(2-furyl)-2-oxobutenoic acid sodium salt on a nickel catalyst has been studied. Using Raney nickel catalyst, the corresponding salts of 4-(2-furyl)-2-oxobutanoic acid, 4-(2-furtyl)-2-hydroxybutanoic acid, and aliphatic hydrogenolysis products of the initial compound were obtained. The sodium salt of 2-hydroxy-4-(2-tetrahydrofuryl) butanoic acid and the condensation product 4-(2-furylethyl)-3-(2-furylmethyl)-2-oxo-3,4-didehydroglutaric acid were detected in the hydrogenolysate. A method has been developed for obtaining the sodium salts of 4-(2-furyl)-2-oxobutanoic and 4-(2-furyl)-2-hydroxybutanoic acids.

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References

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Authors
  1. V. A. Slavinskaya
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  2. D. É. Sile
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  3. M. Yu. Katkevich
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  4. É. Kh. Korchagova
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  5. N. G. Panchenko
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  6. I. U. Lipsbergs
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  7. E. Lukevics
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Additional information

Latvian Institute of Organic Synthesis, Riga LV-1006, e-mail: elmira@osi.lanet.lv. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 1, pp. 41–45, January, 1998.

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Slavinskaya, V.A., Sile, D.É., Katkevich, M.Y. et al. Hydrogenation of 4-(2-furyl)-2-oxobutenoic acid sodium salt on Raney nickel. Chem Heterocycl Compd 34, 35–39 (1998). https://doi.org/10.1007/BF02290609

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  • DOI: https://doi.org/10.1007/BF02290609

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