Chromatographia

, Volume 15, Issue 2, pp 125–132 | Cite as

Fast analysis by gas chromatography

  • G. Gaspar
  • C. Vidal-Madjar
  • G. Guiochon
Originals

Summary

The efficiency of fast GC columns depends largely on the quality of the chromatograph. A theoretical and experimental study shows the relative importance of the various phenomena involved and permits the optimization of a GC System. Extremely good performances, exceeding 2,500 plates per second have been routinely obtained.

Key Words

Capillary columns Fast analysis Gas chromatography Instrumental effects Optimization 

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References

  1. [1]
    G. Gaspar, P. Arpino, G. Guiochon, J. Chromatogr. Sci.15, 256–261 (1977).Google Scholar
  2. [2]
    R. Annino, J. Leone, to be published.Google Scholar
  3. [3]
    G. Guiochon, Advances in chromatography,J. C. Giddings, R. A. Keller (Eds.), Dekker, New York, 1969, Vol. 8, p. 179.Google Scholar
  4. [4]
    M. J. E. Golay, Gas chromatography (1957),V. J. Coates, H. J. Noebels, I. S. Fagerson (Eds.), Academic Press, New York 1958, p. 1.Google Scholar
  5. [5]
    J. C. Giddings, P. D. Schettler, Anal. Chem.36, 1483 (1964).Google Scholar
  6. [6]
    G. Gaspar, R. Annino, C. Vidal-Madjar, G. Guiochon Anal. Chem.50, 1512 (1978).Google Scholar
  7. [7]
    J. C. Sternberg, Advances in chromatography,J.J. Giddings R. A. Keller (Eds.), Dekker, New York, 1966, Vol. 2, p. 205.Google Scholar
  8. [8]
    G. Guiochon, J. Chromatogr.185, 3 (1979).Google Scholar
  9. [9]
    J. J. Giddings, in Chromatography,E. Heftmann (Ed.), Van Nostrand, New York, 3rd ed., 1975, p. 27.Google Scholar
  10. [10]
    R. P. W. Scott, G. S. F. Hazeldean, in Gas Chromatography 1960,R. P. W. Scott (Ed.), Butterworths, London, 1960, p. 144.Google Scholar
  11. [11]
    I. Halasz, K. Hartman, E. Heine, Gas Chromatography 1964A. Goldup (Ed.), The Institute of Petroleum, London, 1964 p. 38.Google Scholar
  12. [12]
    D. V. Grant, J. Chromatogr.122, 107 (1976).Google Scholar
  13. [13]
    E. Grushka, Anal. Chem.44, 1733 (1972).Google Scholar
  14. [14]
    O. Grubner, Adv. Chromatogr.6, 173 (1968).Google Scholar
  15. [15]
    G. Gaspar, J. P. Olivo, G. Guiochon, Chromatographia 11. 321 (1978).Google Scholar
  16. [16]
    I. Halasz, G. Schreyer, Chem. Ing. Tech.32, 675 (1960).Google Scholar
  17. [17]
    D. H. Desty, A. Goldup, in Gas Chromatography 1960.R. P. W. Scott (Ed.), Butterworths, London, 1960, pp. 162.Google Scholar
  18. [18]
    J. L. Di Cesare, M. W. Dong, L. S. Ettre, Chromatographia14, 257 (1981).Google Scholar
  19. [19]
    D. H. Desty, Advances in Chromatography,J. C. Giddings R. A. Keller (Eds.), Dekker, New York, 1965, Vol. 1, p. 199.Google Scholar

Copyright information

© Friedr. Vieweg & Sohn Verlagsgesellschaft mbH 1982

Authors and Affiliations

  • G. Gaspar
    • 1
  • C. Vidal-Madjar
    • 2
  • G. Guiochon
    • 2
  1. 1.Department of Physical ChemistryTechnical University of BudapestH-BudapestHungary
  2. 2.Laboratoire de Chimie Analytique PhysiqueEcole PolytechniquePalaiseau CedexFrance

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