Advertisement

Chromatographia

, Volume 9, Issue 10, pp 520–522 | Cite as

Capillary gas chromatography of hypnotics, methyprylon (noludarR) and pyrithyldion (persedonR), after derivatization in an all glass solid injector

  • M. Lauwereys
  • A. Vercruysse
Short Communications

Summary

The possibility of forming silyl derivatives of methyprylon and pyrithyldion following an alternative and time-saving procedure is discussed. The derivatives are formed on the needle tip of an all glass solid injector. The linearity and reproduciblity of their gas chromatographic behaviour on a capillary column is tested over a concentration range of 0.5 μg −2.5 μg.

Keywords

Chromatography Analytical Chemistry Organic Chemistry Capillary Column Silyl 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. [1]
    Van den Berg, P. M. J., Th. P. H. Cox, Chromatographia5, 301 (1972).Google Scholar
  2. [2]
    Luyten, J. A., G. A. Rutten, J. Chromatogr.91, 393 (1974).Google Scholar
  3. [3]
    Alexander, G., G. A. Rutten, J. Chromatogr.99, 81 (1974).Google Scholar
  4. [4]
    Franken, J. J., M. M. Trijbels, J. Chromatogr.91, 425 (1974).Google Scholar

Copyright information

© Friedr. Vieweg & Sohn, Verlagsgesellschaft mbH 1976

Authors and Affiliations

  • M. Lauwereys
    • 1
  • A. Vercruysse
    • 1
  1. 1.Department of Pharmacognosy, Phytochemistry and ToxicologyVrije Universiteit BrusselSint Genesius-RodeBelgium

Personalised recommendations