Skip to main content
Log in

Determination of unpolymerized methyl methacrylate in contact lenses by headspace gas chromatography

  • Short Communications
  • Published:
Chromatographia Aims and scope Submit manuscript

Summary

A modified gas chromatographic method is described for the determination of free monomer in contact lenses, irrespective of the method of production. It thus becomes possible to assess very quickly the conformity of such lenses with hygiene regulations. This method allows direct supervision of production or determination of the quality of a product of unknown origin in only 15 min. Production tests of new polymerization initiators, reactors for polymerization, etc. can also be carried out.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

References

  1. U.S. Pat. No. 3728317 (1973).

  2. U.S. Pat. No. 4123408 (1978).

  3. U.S. Pat. No. 3808179 (1974).

  4. E. Malten, R. Wigwers, J. A. C. J.5, 178 (1979).

    Google Scholar 

  5. H. Proctor, J. Hughes, Chemical Hazards of the Workplace, 239 Philadelphia, 1978, p. 89.

    Google Scholar 

  6. A Guide to Health and Safety in GRP-Fabrication, Executive HMSO Publ. Centre, London, 1987, p. 79.

  7. W. Arens, C. Siegert, Gas und Wasserfach98, 661 (1957).

    Google Scholar 

  8. S. Chanceller, Nature185, 841 (1960).

    Google Scholar 

  9. H. Raymond, A. Pierson, Anal. Chem.,28, 1213 (1956)

    Google Scholar 

  10. A. Rijeke, A. Johnson, E. Oster, J. Biol. Mafer. Res.11, 211 (1977).

    Google Scholar 

  11. C. Alley, J. Bocks, G. Choudhary, Anal. Chem.48, 387 (1976).

    Google Scholar 

  12. J. Tanguay, Method Modification for Methyl methacrylate, NIOSH, DPSE, MRSB, unpublished (NIOSH), 1988.

  13. H. Hollefeeld, R. Snyder, C. Breeder, J. Chromatogr. Sci.19, 514 (1981).

    Google Scholar 

  14. B. Kolb, Headspace Gaschromatographie mit Kapillartrennsäulen, Würzburg, 1986, p. 27.

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Tashkov, W., Getchev, V. Determination of unpolymerized methyl methacrylate in contact lenses by headspace gas chromatography. Chromatographia 37, 546–548 (1993). https://doi.org/10.1007/BF02275795

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02275795

Key Words

Navigation