, Volume 7, Issue 3, pp 128–134 | Cite as

Preparation of high resolution nickel open tubular columns

  • W. Bertsch
  • F. Shunbo
  • R. C. Chang
  • A. Zlatkis
Papers Related to Various Aspects of Open Tubular Columms


A detailed description of the production of nickel open tubular columns is given and the important steps are discussed. Two types of surface modification, etching and introduction of a suspended silanized silica, which result in conventional open tubular (COT) and in support coated open tubular (SCOT) columns are described. Properties of these columns are presented for one phase, Emulphor ON 870 and several examples of applications are given.


Nickel Analytical Chemistry Organic Chemistry High Resolution Surface Modification 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.


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  1. [1]
    M. J. E. Golay, “Theory and Practice of Gas-Liquid Partition Chromatography with Coated Capillaries”, in Gas Chromatography (V. J. Coates, H. J. Noebels, andI. S. Fagerson, eds.), Academic Press, New York 1958; p. 1.Google Scholar
  2. [2]
    R. Kaiser, Chromatographie in der Gasphase II, Bibliographisches Institut, Mannheim, 1966.Google Scholar
  3. [3]
    L. S. Ettre, Open Tubular Columns in Gas Chromatography. Plenum Press, New York, 1965.Google Scholar
  4. [4]
    G. Guiochon, “Comparison of the Performances of the Various Column Types Used in Gas Chromatography”, in Advances in Chromatography Vol. 8 (J. C. Giddings andR. A. Keller, eds.), M. Dekker Inc., New York, 1969; p. 179.Google Scholar
  5. [5]
    M. Novotný andA. Zlatkis, Chromatog. Rev.14, 1 (1971).CrossRefGoogle Scholar
  6. [6]
    D. H. Desty, A. Goldup, B. H. F. Whyman, J. Inst. Petrol.45, 287 (1959).Google Scholar
  7. [7]
    R. Kaiser, ref. [2] p. 132.Google Scholar
  8. [8]
    A. Zlatkis, “Ionization Detectors and Capillary Columns”, in Lectures on Gas Chromatography 1962 (H. A. Szymanski, ed.), Plenum Press, New York, 1963; p. 87.Google Scholar
  9. [9]
    A. Zlatkis andJ. Q. Walker, Anal. Chem.35, 1359 (1963).CrossRefGoogle Scholar
  10. [10]
    K. Grob, Mittlg. Geb. Lebensmittelunt. Hyg.63, (10), 23 (1972).Google Scholar
  11. [11]
    D. L. Petitjean, andC. J. Leftault, Jr., J. Gas Chromatog.,1 (3), 18 (1963).Google Scholar
  12. [12]
    R. P. W. Scott, Nature183, 1753 (1959).Google Scholar
  13. [13]
    D. C. Fenimore, Private communication.Google Scholar
  14. [14]
    A. Zlatkis, H. A. Lichtenstein, andA. Tishbee, Chromatographia6, 67 (1973).CrossRefGoogle Scholar
  15. [15]
    M. Blumer, Anal. Chem.45, 980 (1973).CrossRefGoogle Scholar

Copyright information

© Friedr. Vieweg & Sohn, Verlagschesellschaft mbH 1974

Authors and Affiliations

  • W. Bertsch
    • 1
  • F. Shunbo
    • 1
  • R. C. Chang
    • 1
  • A. Zlatkis
    • 1
  1. 1.Department of ChemistryUniversity of HoustonHoustonU.S.A.

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