Summary
A new method is proposed for the analysis by gas chromatography of volatile compounds found in alcoholic and acetic fermentation samples.
The method represents a suitable choice for the accurate and precise determination of 19 compounds (including Methanol) by direct injection onto a single column.
Chromatograms of synthetic mixtures as well as actual samples show the capabilities of the micropacked column used.
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References
A. C. Noble, R. A. Flath, R. R. Forrey, J. Agric. Food Chem.,28, 346 (1980).
M. D. Cabezudo, M. C. Polo, M. Herraiz, G. Reglero, M. González Raurich, I. Cáceres, P. Martín Alvarez, in “The Shelf Life of Foods and Beverages” byG. Charalambous. Ed. Elsevier, Amsterdam 1985, p. 186.
I. Moret, G. Scarponi, P. Cescon, J. Sci. Food Agric.,35, 1004 (1984).
M. C. Polo, M. Herraiz, M. D. Cabezudo, in “Instrumental Analysis of Foods Recent Progress”, byG. Charalambous andG. Inglett. Ed. Academic Press. New York 1983, Vol 2, p. 357.
G. Schomburg, U. Häusig, H. Husmann, HRC & CC,8, 566 (1985).
A. C. Noble, in “Analysis of Food and Beverages. Headspace Techniques” byG. Charalambous. Ed. Academic Press, New York 1978, p. 203.
P. J. Eriksson, in “Aroma of Beer, Wine and Distilled Alcoholic Beverages” byL. Nykänen, H. Suomalainen. Akademie-Verlag, Berlin 1983, p. 322.
F. David, M. Proot, P. Sandra, HRC & CC,8, 551 (1985).
G. Reglero, M. Herraiz, M. D. Cabezudo, E. Fernández Sánchez, J. A. Garcia Domínguez, J. Chromatogr.,348, 327 (1985).
J. Sanz, G. Reglero, M. D. Cabezudo, I. Martínez-Castro, Anal. Chim. Acta 1986 (In press).
A. Bertrand, P. Ribereau-Gayon, Method. Anal. de l'O.I.V., 79/FV/409 bis (1973).
C. Reinhard, Method. Anal. de l'O.I.V., 160/FV/447 (1973).
M. D. Cabezudo, E. F. de Gorostiza, M. Herraiz, J. Fernández Biarge, J. A. Garcia Dominguez, M. J. Molera, J. Chrom. Sci.,16, 61 (1978).
G. Reglero, Doctoral Theses. Universidad Autónoma. Madrid, 1986.
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Reglero, G., Herraiz, T., Herraiz, M. et al. Mixed micropacked columns designed for selective separation of fermentation products. Chromatographia 22, 358–362 (1986). https://doi.org/10.1007/BF02268790
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DOI: https://doi.org/10.1007/BF02268790