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Microcolumn liquid chromatography with silica gel dynamically modified with a bile acid derivative

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Summary

Characteristics of silica gel dynamically modified with a bile acid derivative have been investigated in liquid chromatography. 3-[(3-cholamidopropyl) dimethylamonio]-1-propane-sulfonate (CHAPS) is selected as modifier. CHAPS possesses a quaternary ammonium group which can be attached to the silica gel surface by cation exchange. The stationary phase modified with CHAPS has been applied to the separation of 1,1′-binaphthyl-2,2′-diyl-hydrogen phosphate enantiomers.

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Authors and Affiliations

  1. Faculty of Engineering, Gifu University, 1-1 Yanagido, Gifu, 501-11, Japan

    T. Takeuchi & T. Miwa

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  1. T. Takeuchi
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  2. T. Miwa
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Dedicated to Professor Leslie S. Ettre on the occasion of his 70th birthday.

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Takeuchi, T., Miwa, T. Microcolumn liquid chromatography with silica gel dynamically modified with a bile acid derivative. Chromatographia 34, 386–390 (1992). https://doi.org/10.1007/BF02268373

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  • DOI: https://doi.org/10.1007/BF02268373

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