Chromatographia

, Volume 18, Issue 9, pp 489–495 | Cite as

Development of capillary supercritical fluid chromatography/Fourier transform infrared spectrometry

  • S. V. Olesik
  • S. B. French
  • M. Novotny
Originals

Summary

The feasibility of a new technique, supercritical fluid chromatography/Fourier transform infrared spectrometry (SFC/FTIR), for separation and identification of nonvolatile and labile compounds in complex mixtures is discussed in this report. The design of a high pressure (flow cell) interface is described. The results of a continuing study of possible mobile phases for SFC/FTIR are presented. Finally, SFC/FTIR was applied to a standard test mixture. The current detection limits of one component of the mixture, 2,6-di-t-butylphenol, are presented.

Key Words

Supercritical Fluid Chromatography (SFC) Infrared Spectrometry (IR or FTIR) Capillary Chromatography 

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Copyright information

© Friedr. Vieweg & Sohn Verlagsgesellschaft mbH 1984

Authors and Affiliations

  • S. V. Olesik
    • 1
  • S. B. French
    • 1
  • M. Novotny
    • 1
  1. 1.Department of ChemistryIndiana UniversityBloomingtonUSA

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