Skip to main content
Log in

Retention parameters of aromatic polar species via reversed-phase liquid chromatography with application to coal liquefaction products

  • Originals
  • Published:
Chromatographia Aims and scope Submit manuscript

Abstract

High performance liquid chromatography in the reversedphase mode was used for the analysis of coal liquefaction materials. The chromatographic system used was optimized for separation of the more polar, heteroatom-containing components. A model study of a wide variety of compounds was undertaken in which capacity factors were correlated to a set of structural parameters in order to gain insight into the retention mechanism. Reversed-phase separation of a model mixture as well as separation of boiling fractions of hydrotreated and nonhydrotreated process recycle solvents are compared.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. D. W. Later, M. L. Lee, K. D. Bartle, R. C. Kong, D. L. Vassilaros, Anal. Chem.53, 1612 (1981).

    Article  Google Scholar 

  2. R. B. Callen, J. G. Bendoraitis, C. A. Simpson, S. E. Voli: Ind. Eng. Chem., Prod. Res. Dev.15, 222 (1976).

    Google Scholar 

  3. M. Farcasiu, Fuel56, 9 (1977).

    Article  Google Scholar 

  4. D. W. Jewell, E. W. Albaugh, E. W. Davis, R. G. Rubuto Ind. Eng. Chem. Fundam.13, 278 (1974).

    Article  Google Scholar 

  5. S. A. Wise, S. N. Chester, H. S. Hertz, L. R. Hilpert, W. E. May, Anal. Chem.49, 2306 (1977).

    Article  Google Scholar 

  6. J. F. Schabron, R. J. Hurtubise, H. F. Silver, Anal. Chem.49, 2253 (1977).

    Article  Google Scholar 

  7. W. A. Dark, W. H. McFadden, D. L. Bradford, J. Chromatogr. Sci.15, 454 (1977).

    Google Scholar 

  8. J. F. Schabron, R. J. Hurtubise, H. F. Silver, Anal. Chem.51, 1426 (1979).

    Article  Google Scholar 

  9. F. P. Burke, R. A. Winschel, T. C. Pochapsky, Am. Chem. Soc. Div. Fuel Chem. Preprints26 (2), 68 (1981).

    Google Scholar 

  10. J. W. Prather, A. R. Tarrer, J. A. Guin, D. R. Johnson, W. C. Neely, Am. Chem. Soc. Div. Fuel Chem. Preprints21, 144 (1976).

    Google Scholar 

  11. W. A. Dark, W. H. McFadden, J. Chromatogr. Sci.16, 283 (1978).

    Google Scholar 

  12. B. L. Karger, L. R. Snyder, C. Horvath, “An Introduction to Separation Science”, John Wiley & Sons, New York, NY. 1973, p. 388.

    Google Scholar 

  13. L. R. Schronk, R. D. Grigsby, A. R. Hanks, J. Chromatogt. Sci.19, 496 (1981).

    Google Scholar 

  14. M. N. Hasan, P. C. Jurs, Anal. Chem.53, 263 (1983).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Amateis, P.G., Taylor, L.T. Retention parameters of aromatic polar species via reversed-phase liquid chromatography with application to coal liquefaction products. Chromatographia 17, 431–436 (1983). https://doi.org/10.1007/BF02262924

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02262924

Key Words

Navigation