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Low surface area carbonized silica obtained by the pyrolysis of dichloromethane: A column packing for adsorption and exclusion chromatography

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Abstract

Carbonized silica has been used as column packing for HPLC. Up to now it has been obtained by the pyrolysis of the vapour of benzene as well as aliphatic and aromatic alcohols. This paper reports on the properties of carbonized silica obtained by the pyrolysis of dichloromethane and used as column packing in HPLC.

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References

  1. Liquid Column Chromatography — a Survey of Modern Techniques and Applications,Z. Deyl, K. Macek, J. Janák, Eds., Elsevier, Amsterdam, 1975; p. 247.

    Google Scholar 

  2. W. Melander, Cs. Horváth, “Reversed-Phase Chromatography”. In High-Performance Liquid Chromatography,Cs. Horváth, Ed., Academic Press, New York, 1980; Vol. 2, pp. 114–319.

    Google Scholar 

  3. L. R. Snyder, J. J. Kirkland, Introduction to Modern, Liquid Chromatography, John Wiley & Sons, New York, 2nd ed., 1979; p. 173.

    Google Scholar 

  4. H. Colin, C. Eon, G. Guiochon, J. Chromatogr.119, 41 (1976).

    Google Scholar 

  5. N. K. Bebris, A. V. Kiselev, Yu. S. Nikitin, J. J. Frolov, L. V. Tarasowa, Ya. J. Yashin, Chromatographia11, 206 (1978).

    Google Scholar 

  6. R. Leboda, A. Waksmundzki, A. Gierak, Z. Suprynowicz, Chem. Anal.22, 603 (1977).

    Google Scholar 

  7. R. Leboda, A. Waksmundzki, J. Suprynowicz, M. Waksmundzka-Hajnos, Chem. Anal.21, 165 (1976).

    Google Scholar 

  8. R. Leboda, A. Waksmundzki, J. Skubiszewska, Z. Suprynowicz, Chem. Anal.23, 397 (1978).

    Google Scholar 

  9. K. Grob, Helv. Chim. Acta,48, 1362 (1965).

    Google Scholar 

  10. R. Leboda Chem. Anal., in press.

  11. R. Leboda, Chem. Anal. 25 (1980).

  12. A. Gierak, A. Waksmundzki, B. Buszewski, R. Lodkowski, Chem. Anal.26, 93 (1981).

    Google Scholar 

  13. A. Waksmundzki, B. Ościk-Mendyk, A. Dawidowicz, Chem. Anal.24, 667 (1979).

    Google Scholar 

  14. P. Jandera, M. Janderowa, J. Churacek, J. Chromatogr.149, 79 (1978).

    Google Scholar 

  15. H. Colin, G. Guiochon, J. Chromatogr.126, 43 (1976).

    Google Scholar 

  16. N. K. Bebris, R. G. Vorobieva, A. V. Kiselev, Yu. S. Nikitin, L. V. Tarasowa, J. J. Frolov, Ya. J. Yashin, J. Chromatogr.117, 257 (1976).

    Google Scholar 

  17. R. Leboda, Crbonized Silica as Chromatographic Adsorbents: Their Preparation and Properties. Ph. D. Thesis, Maria Curie Sklodowska University, Lublin, 1980.

    Google Scholar 

  18. G. Glöckner, Polymercharakterisierung durch Flüssigkeitschromatographie, VEB Deutscher Verlag der Wissenschaften, Berlin 1980; pp. 128–194.

    Google Scholar 

  19. A. Dawidowicz, S. Sokolowski, J. Chromatogr.125, 428 (1976).

    Google Scholar 

  20. R. Leboda, Chromatographia,13, 703 (1980).

    Google Scholar 

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Dawidowicz, A.L., Gierak, A. & Waksmundzki, A. Low surface area carbonized silica obtained by the pyrolysis of dichloromethane: A column packing for adsorption and exclusion chromatography. Chromatographia 17, 627–632 (1983). https://doi.org/10.1007/BF02261947

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  • DOI: https://doi.org/10.1007/BF02261947

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