Summary
A reaction detector with non-segmented flow in open tubes as reaction track is described. To minimize peak broadening the open tubes are arranged in a three dimensional coiled structure by knitting. At low volume flow rates the h-values in these open tubes are independent of flow rate and are significantly lower than predicted by theory. The applicability of this reactor for classical colorimetric detection with corrosive reagents is shown.
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Part of Ph. D. Thesis, Saarbrücken 1976
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Engelhardt, H., Neue, U.D. Reaction detector with three dimensional coiled open tubes in HPLC. Chromatographia 15, 403–408 (1982). https://doi.org/10.1007/BF02261598
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DOI: https://doi.org/10.1007/BF02261598