Summary
A new method was developed for the determination of fluoride in fluorinated milk on the basis of headspace gas chromatography utilizing, the reaction between trimethylchlorosilane and ion-bound fluorine in highly acidic media. The obtained trifluorosilane has a high volatility and can be easily determined by headspace gas chromatography.
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References
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Tashkov, W., Benchev, I., Rizov, N. et al. Fluoride determination in fluorinated milk by headspace gas chromatography. Chromatographia 29, 544–546 (1990). https://doi.org/10.1007/BF02261219
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DOI: https://doi.org/10.1007/BF02261219