Summary
The pungent principles of ginger and grains of paradise are examined using a reversed-phase HPLC column. An electrochemical detector is used to selectively detect the phenolic gingerols and shogaols. The retention indices of the compounds are compared using methanowater and acetonitrile-water as eluents.
References
R. M. Smith, J. M. Robinson, Phytochemistry20, 203 (1981).
D. J. Harvey, J. Chromatogr.212, 75 (1981).
P. Denniff, I. Macleod, D. H. Whiting, J. Chem. Soc., PerkinI, 82 (1981).
D. W. Connell, R. McLachlan, J. Chromatogr.67, 29 (1972).
D. W. Connell, Flavour Industry, 677 (1970).
V. S. Govindarajan, S. Narasimham, B. Rajalakshmi, D. Rajalakshmi, Z. Lebensm. Unters. Forsch.170, 200 (1980).
A preliminary report of the work has been presented by R. M. Smith, at the 5th Anglo-Czech Symposium on Electrochemistry and a report will appear in “Fundamental Aspects and Analytical Applications of Electrochemistry Detectors”, Ed.T. Ryan, Plenum Press, in press.
D. W. Connell, Aust. J. Chem.23, 369 (1970).
E. L. Johnson, R. E. Majors, L. Werum, P. Reiche, “Liquid Chromatographic analysis of Food and Beverages”, Volume 1, Ed.G. Charalambous, Academic Press, New York, N.Y. (1979).
J. E. Woodbury, J. Assoc. Off. Anal. Chem.63, 556 (1980).
A. Saria, F. Lembeck, G. Skofitsch, J. Chromatogr.208, 41 (1981).
R. M. Smith, J. Chromatogr.236, 313 (1982).
R. M. Smith, J. Chromatogr.236, 321 (1982).
D. W. Connell Aust. J. Chem.23, 369 (1970).
E. Steinegger, K. Stuki, Pharm. Acta Helv.,57, 66 (1982).
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Smith, R.M. Analysis of the pungent principles of ginger and grains of paradise by high-performance liquid chromatography using electrochemical detection. Chromatographia 16, 155–157 (1982). https://doi.org/10.1007/BF02258887
Received:
Accepted:
Issue Date:
DOI: https://doi.org/10.1007/BF02258887