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Determination of elemental composition of aluminosilicate clays by EDXRF

  • J. Hanif
  • I. Hanif
Article

Abstract

Aluminosilicate clay samples were analyzed for the constituent elements with respect to a certified reference material using microcrystalline cellulose powder as a binder for presentation as a pressed pellet to an energy dispersive X-ray fluorescence spectrometer. Sample preparation for presentation is highlighted. The data manipulation to achieve the analytical accuracy from the inherent precision is discussed.

Keywords

Cellulose Sample Preparation Reference Material Elemental Composition Aluminosilicate 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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References

  1. 1.
    F. SINGER, S. S. SINGER, Industrial Ceramics, Chapman and Hall, 1978, p. 300.Google Scholar
  2. 2.
    J. B. KRAUSE, L. H. BARTON, Adv. X-Ray Anal., 21 (1977) 71.Google Scholar
  3. 3.
    R. C. HAGAN, Report LA-9400-MS, USA, 1982.Google Scholar
  4. 4.
    J. PESCUAL, Talanta, 34, 12 (1978) 1027.Google Scholar
  5. 5.
    B. S. KING, L. F. ESPOS, B. P. FABBI, Adv. X-ray Anal, 21 (1977) 75.Google Scholar
  6. 6.
    E. P. BERTIN, Introduction to X-ray Spectrometric analysis, Plenum Press, New York, 1978.Google Scholar
  7. 7.
    R. TERTIAN, F. CLAISSE, Principals of Quantitative X-ray Fluorescence Analysis, Heyden, London, 1982.Google Scholar
  8. 8.
    J. C. RUSS, Fundamentals of Energy Dispersive X-ray Analysis, Butterworth, London, 1984.Google Scholar
  9. 9.
    P. J. STATHAM, Anal. Chem., 49 (1977) 2149.Google Scholar
  10. 10.
    P. J. STATHAM, J. Microscopy, 123 (1981) 1.Google Scholar
  11. 11.
    Links systems, XR-500, User's Manual, SR2-500-XRF-0583, Halifax Road, Bucks, U.K.Google Scholar
  12. 12.
    Links Systems, XFF/FLS Operating Instructions, XRF-500-XFF-0984, Halifax Road, Bucks, U.K.Google Scholar
  13. 13.
    R. THIESEN, D. VOLLATH, Tables of X-ray Mass Attenuation Coefficients, Verlag Stahleisen, Dusseldorf, 1967.Google Scholar
  14. 14.
    Links System, Data Slide, Perrygraph Div. Nashua Corp., USA, 1984.Google Scholar
  15. 15.
    J. SHERMAN, Spectrochim. Acta, 7 (1955) 283.Google Scholar
  16. 16.
    S. D. RASBERRY, K. F. J. HEINRICH, Anal. Chem., 46 (1974) 81.Google Scholar
  17. 17.
    C. J. SPARKS Jr., Adv. X-Ray Anal., (1976) 19.Google Scholar
  18. 18.
    B. VREBOS, J. A. HELSEN, X-Ray Spectrom, 14 (1985) 27.Google Scholar
  19. 19.
    P. VAN ESPAN, H. NULLEN, F. ADAMS, Proc. of A.N.S. Topical Conf., D.O.E. Pub. CONF-78042. 1978, p. 96.Google Scholar
  20. 20.
    N. S. SALEH, K. A. AL-SALEH, A. J. ABU EL-HAIJA, J. Radioanal. Nucl. Chem., 120 (1988) 161.Google Scholar
  21. 21.
    R. A. VANE, Adv. X-ray Anal., 26 (1982) 369.Google Scholar
  22. 22.
    D. A. GEDCKE, L. G. BYARS, N. C. JACOBUS, Adv. X-ray Anal., 26 (1982) 355.Google Scholar
  23. 23.
    F. SINGER, S. S. SINGER, Industrial Ceramics, Chapman and Hall, London, 1978, p. 24.Google Scholar
  24. 24.
    W. BAUMGART, A. C. DUNHAM, G. C. AMMSTUTZ, Process Mineralogy of Ceramic Materials, Ferdinand Enke Publishers, Stuttgart, 1984.Google Scholar
  25. 25.
    R. CAULCUTT, R. BUDDY, Statistics for Analytical Chemists, Chapman and Hall, London, 1983.Google Scholar

Copyright information

© Akadémiai Kiadó 1993

Authors and Affiliations

  • J. Hanif
    • 1
  • I. Hanif
    • 1
  1. 1.Pakistan Institute of Nuclear Science and TechnologyIslamabad(Pakistan)

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